CH((CMe)(2,6-(i)Pr₂C₆H₃N))2GeP(H)SiMe₃

Base Information

Chemical Name:CH((CMe)(2,6-(i)Pr₂C₆H₃N))2GeP(H)SiMe₃
CAS No.:1040234-85-2
Molecular Formula:C₃₂H₅₁GeN₂PSi
Molecular Weight:595.42
Hs Code.:

CH((CMe)(2,6-(i)Pr<sub>2</sub>C<sub>6</sub>H<sub>3</sub>N))2GeP(H)SiMe<sub>3</sub>

Synonyms:CH((CMe)(2,6-(i)Pr₂C₆H₃N))2GeP(H)SiMe₃

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Chemical Property of CH((CMe)(2,6-(i)Pr₂C₆H₃N))2GeP(H)SiMe₃

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Technology Process of CH((CMe)(2,6-(i)Pr₂C₆H₃N))2GeP(H)SiMe₃

There total 2 articles about CH((CMe)(2,6-(i)Pr₂C₆H₃N))2GeP(H)SiMe₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 27607-77-8
trimethylsilyl trifluoromethanesulfonate

: 1040234-81-8
CH((CMe)(2,6-(i)Pr₂C₆H₃N))2GePH₂

: 1040234-85-2
CH((CMe)(2,6-(i)Pr₂C₆H₃N))2GeP(H)SiMe₃

Guidance literature:: With triethylamine; In diethyl ether; under N2 atm. to cooled (-60°C) soln. Ge complex in Et2O and Et3NTfOSiMe3 was added dropwise and stirred for 2 h, react. mixt. was allow ed to warm slowly to room temp. and stirred overnight; volatiles were removed in vacuo, residue was extd. with n-hexane, concd.and stored at -20°C for 2 days; elem. anal.;
DOI:10.1021/om800269f

Reference yield:

: 334719-93-6
[C₃H(CH₃)2(N(2,6-diisopropylphenyl))2 chlorogermylene]

: 1040234-85-2
CH((CMe)(2,6-(i)Pr₂C₆H₃N))2GeP(H)SiMe₃

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: triethylamine / diethyl ether

With triethylamine; In diethyl ether;
DOI:10.1021/om800269f