CC-223

Base Information

Chemical Name:CC-223
CAS No.:1441766-23-9
Molecular Formula:C₂₁H₂₇N₅O₃
Molecular Weight:399.466
Hs Code.:

Synonyms:CC-223

Suppliers and Price of CC-223

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Chemical Property of CC-223

Chemical Property:

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Technology Process of CC-223

There total 8 articles about CC-223 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1228014-09-2
7-bromo-1-((1r,4r)-4-methoxycyclohexyl)-3,4-dihydropyrazino[2,3-b]pyrazin-2(1H)-one

: C₁₃⁽¹⁴⁾CH₂₂BNO₃*(x)ClH

: 1441766-23-9
CC-223

Guidance literature:: With bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); potassium carbonate; In tetrahydrofuran; water; at 70 - 75 ℃; for 16h; Sealed tube;

Reference yield:

: 1228013-60-2
ethyl-2-(3,5-dibromopyrazin-2-ylamino)acetate

: 1441766-23-9
CC-223

Guidance literature:: Multi-step reaction with 3 steps

1: 1-methyl-pyrrolidin-2-one / 125 - 130 °C / Large scale

2: phosphoric acid / water / 80 °C / Large scale

3: bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); potassium carbonate / tetrahydrofuran; water / 16 h / 70 - 75 °C / Sealed tube

With bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); phosphoric acid; potassium carbonate; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; water;

Reference yield:

: 1441765-92-9
C₇⁽¹⁴⁾CH₁₀BrNO

: 1441766-23-9
CC-223

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / dichloromethane / 18 h / 20 °C

2: potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / 1,4-dioxane / 18 h / 90 °C

3: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C / Inert atmosphere

4: bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); potassium carbonate / tetrahydrofuran; water / 16 h / 70 - 75 °C / Sealed tube

With hydrogenchloride; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; bis(di-tert-?butyl(4-?dimethylaminophenyl)?phosphine)?dichloropalladium(II); potassium acetate; potassium carbonate; triethylamine; In tetrahydrofuran; 1,4-dioxane; dichloromethane; water;