(S)-N-tert-butoxy-N-1'-(1''-naphthyl)ethyl (R)-2-benzyloxypent-4-enamide

Base Information

Chemical Name:(S)-N-tert-butoxy-N-1'-(1''-naphthyl)ethyl (R)-2-benzyloxypent-4-enamide
CAS No.:1234714-03-4
Molecular Formula:C₂₈H₃₃NO₃
Molecular Weight:431.575
Hs Code.:

Synonyms:(S)-N-tert-butoxy-N-1'-(1''-naphthyl)ethyl (R)-2-benzyloxypent-4-enamide

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Chemical Property of (S)-N-tert-butoxy-N-1'-(1''-naphthyl)ethyl (R)-2-benzyloxypent-4-enamide

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Technology Process of (S)-N-tert-butoxy-N-1'-(1''-naphthyl)ethyl (R)-2-benzyloxypent-4-enamide

There total 1 articles about (S)-N-tert-butoxy-N-1'-(1''-naphthyl)ethyl (R)-2-benzyloxypent-4-enamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1234713-87-1
(S)-N-tert-butoxy-N-1'-(1''-naphthyl)ethyl 2-benzyloxyacetamide

: 106-95-6
allyl bromide

: 1234714-03-4
(S)-N-tert-butoxy-N-1'-(1''-naphthyl)ethyl (R)-2-benzyloxypent-4-enamide

Guidance literature:: (S)-N-tert-butoxy-N-1'-(1''-naphthyl)ethyl 2-benzyloxyacetamide; With 18-crown-6 ether; potassium hexamethylsilazane; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

allyl bromide; In tetrahydrofuran; at -78 ℃; optical yield given as %de; diastereoselective reaction;
DOI:10.1016/j.tet.2010.03.105

Reference yield: 98.0%

: 1234714-03-4
(S)-N-tert-butoxy-N-1'-(1''-naphthyl)ethyl (R)-2-benzyloxypent-4-enamide

: 1177266-30-6
C₁₆H₂₁NO

: 80928-05-8,137819-87-5
(R)-(+)-2-Benzyloxybutyraldehyde

Guidance literature:: (S)-N-tert-butoxy-N-1'-(1''-naphthyl)ethyl (R)-2-benzyloxypent-4-enamide; With lithium aluminium tetrahydride; In tetrahydrofuran; at -15 ℃; Inert atmosphere;

In tetrahydrofuran; at 0 ℃; pH=7; phosphate buffer;
DOI:10.1016/j.tet.2010.03.105

Reference yield: 93.0%

: 1234714-03-4
(S)-N-tert-butoxy-N-1'-(1''-naphthyl)ethyl (R)-2-benzyloxypent-4-enamide

: 1177266-30-6
C₁₆H₂₁NO

: 159622-96-5
(R)-(+)-2-Benzyloxypent-4-enal

Guidance literature:: (S)-N-tert-butoxy-N-1'-(1''-naphthyl)ethyl (R)-2-benzyloxypent-4-enamide; With lithium aluminium tetrahydride; In tetrahydrofuran; at -15 ℃; Inert atmosphere;

In tetrahydrofuran; at 0 ℃; pH=7; phosphate buffer;
DOI:10.1016/j.tet.2010.03.105