(1R,5S,8S)-2-(4-tert-Butylphenyl)-8-phenyl-3,7-dioxa-2-azabicyclo<3.3,0>octan

Base Information

Chemical Name:(1R,5S,8S)-2-(4-tert-Butylphenyl)-8-phenyl-3,7-dioxa-2-azabicyclo<3.3,0>octan
CAS No.:134180-59-9
Molecular Formula:C₂₁H₂₅NO₂
Molecular Weight:323.435
Hs Code.:

Synonyms:(1R,5S,8S)-2-(4-tert-Butylphenyl)-8-phenyl-3,7-dioxa-2-azabicyclo<3.3,0>octan

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Chemical Property of (1R,5S,8S)-2-(4-tert-Butylphenyl)-8-phenyl-3,7-dioxa-2-azabicyclo<3.3,0>octan

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Technology Process of (1R,5S,8S)-2-(4-tert-Butylphenyl)-8-phenyl-3,7-dioxa-2-azabicyclo<3.3,0>octan

There total 3 articles about (1R,5S,8S)-2-(4-tert-Butylphenyl)-8-phenyl-3,7-dioxa-2-azabicyclo<3.3,0>octan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 134180-62-4
(S)-(+)-2-Phenyl-3-oxa-5-hexensaeure-ethylester

: 134180-59-9
(1R,5S,8S)-2-(4-tert-Butylphenyl)-8-phenyl-3,7-dioxa-2-azabicyclo<3.3,0>octan

Guidance literature:: Multi-step reaction with 2 steps

1: diisobutylaluminum hydride / diethyl ether; hexane / 1 h / -78 °C

2: MgSO₄ / diethyl ether / 1a) 0 deg C, 2 h, b) r. t., 18 h

With diisobutylaluminium hydride; magnesium sulfate; In diethyl ether; hexane;

Reference yield:

: 13704-09-1
(S)-(-)-ethyl mandelate

: 134180-59-9
(1R,5S,8S)-2-(4-tert-Butylphenyl)-8-phenyl-3,7-dioxa-2-azabicyclo<3.3,0>octan

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / MgSO₄, Ag₂O / petroleum ether / 18 h / Ambient temperature

2: diisobutylaluminum hydride / diethyl ether; hexane / 1 h / -78 °C

3: MgSO₄ / diethyl ether / 1a) 0 deg C, 2 h, b) r. t., 18 h

With diisobutylaluminium hydride; magnesium sulfate; silver(l) oxide; In diethyl ether; hexane; Petroleum ether;