(1'R,3'R)-2-(3'-hydroxy-2',2'-dimethyl-6'-methylene-cyclohexyl)-ethyl trimethylacetate

Base Information

Chemical Name:(1'R,3'R)-2-(3'-hydroxy-2',2'-dimethyl-6'-methylene-cyclohexyl)-ethyl trimethylacetate
CAS No.:183903-01-7
Molecular Formula:C₁₆H₂₈O₃
Molecular Weight:268.397
Hs Code.:

Synonyms:(1'R,3'R)-2-(3'-hydroxy-2',2'-dimethyl-6'-methylene-cyclohexyl)-ethyl trimethylacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1'R,3'R)-2-(3'-hydroxy-2',2'-dimethyl-6'-methylene-cyclohexyl)-ethyl trimethylacetate

Chemical Property:

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Technology Process of (1'R,3'R)-2-(3'-hydroxy-2',2'-dimethyl-6'-methylene-cyclohexyl)-ethyl trimethylacetate

There total 1 articles about (1'R,3'R)-2-(3'-hydroxy-2',2'-dimethyl-6'-methylene-cyclohexyl)-ethyl trimethylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 2,2-Dimethyl-propionic acid (E)-6-((R)-3,3-dimethyl-oxiranyl)-4-trimethylsilanylmethyl-hex-3-enyl ester

: 183903-01-7
(1'R,3'R)-2-(3'-hydroxy-2',2'-dimethyl-6'-methylene-cyclohexyl)-ethyl trimethylacetate

: 183728-39-4
(1'S,3'R)-2-(3'-hydroxy-2',2'-dimethyl-6'-methylene-cyclohexyl)-ethyl trimethylacetate

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; at -78 ℃; for 1h;
DOI:10.1016/0957-4166(96)00391-6

Reference yield:

: 183903-01-7
(1'R,3'R)-2-(3'-hydroxy-2',2'-dimethyl-6'-methylene-cyclohexyl)-ethyl trimethylacetate

: 1005-56-7
phenylcarbonochloridothioate

: 2,2-Dimethyl-propionic acid 2-((1R,3R)-2,2-dimethyl-6-methylene-3-phenoxythiocarbonyloxy-cyclohexyl)-ethyl ester

Guidance literature:: With pyridine; In dichloromethane; at 25 ℃; for 4h;
DOI:10.1016/0957-4166(96)00391-6

Reference yield:

: 183903-01-7
(1'R,3'R)-2-(3'-hydroxy-2',2'-dimethyl-6'-methylene-cyclohexyl)-ethyl trimethylacetate

: 112243-60-4
(1'S)-2-(2',2'-dimethyl-6'-methylene-cyclohexyl)-ethanol

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / CH₂Cl₂ / 4 h / 25 °C

2: AIBN, n-Bu₃SnH / tetrahydrofuran / 5 h / Heating

3: LiEt₃BH / tetrahydrofuran / 2 h / Heating

With pyridine; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; lithium triethylborohydride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/0957-4166(96)00391-6