Phosphoric acid bis-(2-cyano-ethyl) ester 1-(2-nitro-phenyl)-ethyl ester

Base Information

Chemical Name:Phosphoric acid bis-(2-cyano-ethyl) ester 1-(2-nitro-phenyl)-ethyl ester
CAS No.:144758-79-2
Molecular Formula:C₁₄H₁₆N₃O₆P
Molecular Weight:353.271
Hs Code.:

Synonyms:Phosphoric acid bis-(2-cyano-ethyl) ester 1-(2-nitro-phenyl)-ethyl ester

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Chemical Property of Phosphoric acid bis-(2-cyano-ethyl) ester 1-(2-nitro-phenyl)-ethyl ester

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Technology Process of Phosphoric acid bis-(2-cyano-ethyl) ester 1-(2-nitro-phenyl)-ethyl ester

There total 4 articles about Phosphoric acid bis-(2-cyano-ethyl) ester 1-(2-nitro-phenyl)-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₄H₁₆N₃O₅P

: 144758-79-2
Phosphoric acid bis-(2-cyano-ethyl) ester 1-(2-nitro-phenyl)-ethyl ester

Guidance literature:: With tert.-butylhydroperoxide; at -40 ℃; for 1h;
DOI:10.1039/c8sc01233d

Reference yield:

: 80379-10-8,108530-03-6,142631-59-2,3205-25-2
1-(2-nitrophenyl)ethan-1-ol

: 102690-88-0
bis(2-cyanoethyl) diisopropylamidophosphite

: 144758-79-2
Phosphoric acid bis-(2-cyano-ethyl) ester 1-(2-nitro-phenyl)-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1H-tetrazole / acetonitrile / 20 °C

2: tert.-butylhydroperoxide / 1 h / -40 °C

With 1H-tetrazole; tert.-butylhydroperoxide; In acetonitrile;
DOI:10.1039/c8sc01233d

Reference yield:

: 102690-88-0
bis(2-cyanoethyl) diisopropylamidophosphite

: 3205-25-2,108530-03-6,142631-59-2,80379-10-8
(S)-1-(2-nitrophenyl)ethanol

: 144758-79-2
Phosphoric acid bis-(2-cyano-ethyl) ester (S)-1-(2-nitro-phenyl)-ethyl ester

Guidance literature:: With 1H-tetrazole; 3-chloro-benzenecarboperoxoic acid; Multistep reaction; 1) THF, RT, 1h, 2a) CH₂Cl₂, 0 deg C, 0.5h, 2b) RT, 0.5h;
DOI:10.1039/P19920001015