C₂₈H₄₂O₆

Base Information

Chemical Name:C₂₈H₄₂O₆
CAS No.:950598-42-2
Molecular Formula:C₂₈H₄₂O₆
Molecular Weight:474.638
Hs Code.:

C<sub>28</sub>H<sub>42</sub>O<sub>6</sub>

Synonyms:C₂₈H₄₂O₆

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Chemical Property of C₂₈H₄₂O₆

Chemical Property:

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Technology Process of C₂₈H₄₂O₆

There total 22 articles about C₂₈H₄₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 950598-31-9
C₄₀H₇₀O₆Si₂

: 950598-42-2
C₂₈H₄₂O₆

Guidance literature:: With boron trifluoride diethyl etherate; In methanol; at -78 - 0 ℃; for 3h;
DOI:10.1021/ja073952e

Reference yield:

: 906624-11-1
(3S,6E)-8-(4-methoxybenzyloxy)-2,6-dimethylocta-1,6-dien-3-ol

: 950598-42-2
C₂₈H₄₂O₆

Guidance literature:: Multi-step reaction with 14 steps

1: 97 percent / DCC; DMAP / CH₂Cl₂ / 0 °C

2: 74 percent / [RuCl₂(=CHPh)(PCy₃)(SIMes)] / CH₂Cl₂ / 40 °C

3: DIBALH / CH₂Cl₂ / -78 °C

4: toluene / 80 °C

5: imidazole / CH₂Cl₂

6: DIBALH / CH₂Cl₂ / -78 °C

7: L-(+)-diethyl tartrate; Ti(i-PrO)4; TBHP / molecular sieves 4 Angstroem / CH₂Cl₂ / -20 °C

8: SO₃*pyridine; DMSO; Et₃N / CH₂Cl₂ / -78 - 0 °C

9: 63 percent / LDA / diethyl ether / -78 °C

10: imidazole / CH₂Cl₂

11: DIBALH / CH₂Cl₂ / -78 °C

12: toluene / 80 °C

13: DIBALH / CH₂Cl₂ / -78 °C

14: 97 percent / BF₃*OEt₂ / methanol / 3 h / -78 - 0 °C

With 1H-imidazole; titanium(IV) isopropylate; tert.-butylhydroperoxide; dmap; pyridine-SO₃ complex; diethyl (2R,3R)-tartrate; boron trifluoride diethyl etherate; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; dicyclohexyl-carbodiimide; lithium diisopropyl amide; 4 A molecular sieve; In methanol; diethyl ether; dichloromethane; toluene; 4: Wittig reaction / 7: Sharpless asymmetric epoxidation / 12: Wittig reaction;
DOI:10.1021/ja073952e

Reference yield:

: 906624-08-6
(2R,3S)-2-Iodomethyl-3-[(E)-5-(4-methoxy-benzyloxy)-3-methyl-pent-3-enyl]-2-methyl-oxirane

: 950598-42-2
C₂₈H₄₂O₆

Guidance literature:: Multi-step reaction with 15 steps

1: H₂O

2: 97 percent / DCC; DMAP / CH₂Cl₂ / 0 °C

3: 74 percent / [RuCl₂(=CHPh)(PCy₃)(SIMes)] / CH₂Cl₂ / 40 °C

4: DIBALH / CH₂Cl₂ / -78 °C

5: toluene / 80 °C

6: imidazole / CH₂Cl₂

7: DIBALH / CH₂Cl₂ / -78 °C

8: L-(+)-diethyl tartrate; Ti(i-PrO)4; TBHP / molecular sieves 4 Angstroem / CH₂Cl₂ / -20 °C

9: SO₃*pyridine; DMSO; Et₃N / CH₂Cl₂ / -78 - 0 °C

10: 63 percent / LDA / diethyl ether / -78 °C

11: imidazole / CH₂Cl₂

12: DIBALH / CH₂Cl₂ / -78 °C

13: toluene / 80 °C

14: DIBALH / CH₂Cl₂ / -78 °C

15: 97 percent / BF₃*OEt₂ / methanol / 3 h / -78 - 0 °C

With 1H-imidazole; titanium(IV) isopropylate; tert.-butylhydroperoxide; dmap; pyridine-SO₃ complex; diethyl (2R,3R)-tartrate; boron trifluoride diethyl etherate; water; diisobutylaluminium hydride; dimethyl sulfoxide; triethylamine; dicyclohexyl-carbodiimide; lithium diisopropyl amide; 4 A molecular sieve; In methanol; diethyl ether; dichloromethane; toluene; 5: Wittig reaction / 8: Sharpless asymmetric epoxidation / 13: Wittig reaction;
DOI:10.1021/ja073952e