tert-butyl ((2R,3R)-2-(allyloxy)-4-(N-((S)-1-((4-methoxybenzyl)-oxy)prop-2-yl)-5-nitro-2-(oct-7-en-1-yloxy)benzamido)-3-methylbutyl)(methyl)carbamate

Base Information

Chemical Name:tert-butyl ((2R,3R)-2-(allyloxy)-4-(N-((S)-1-((4-methoxybenzyl)-oxy)prop-2-yl)-5-nitro-2-(oct-7-en-1-yloxy)benzamido)-3-methylbutyl)(methyl)carbamate
CAS No.:1333239-59-0
Molecular Formula:C₄₀H₅₉N₃O₉
Molecular Weight:725.923
Hs Code.:

Synonyms:tert-butyl ((2R,3R)-2-(allyloxy)-4-(N-((S)-1-((4-methoxybenzyl)-oxy)prop-2-yl)-5-nitro-2-(oct-7-en-1-yloxy)benzamido)-3-methylbutyl)(methyl)carbamate

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Chemical Property of tert-butyl ((2R,3R)-2-(allyloxy)-4-(N-((S)-1-((4-methoxybenzyl)-oxy)prop-2-yl)-5-nitro-2-(oct-7-en-1-yloxy)benzamido)-3-methylbutyl)(methyl)carbamate

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Technology Process of tert-butyl ((2R,3R)-2-(allyloxy)-4-(N-((S)-1-((4-methoxybenzyl)-oxy)prop-2-yl)-5-nitro-2-(oct-7-en-1-yloxy)benzamido)-3-methylbutyl)(methyl)carbamate

There total 4 articles about tert-butyl ((2R,3R)-2-(allyloxy)-4-(N-((S)-1-((4-methoxybenzyl)-oxy)prop-2-yl)-5-nitro-2-(oct-7-en-1-yloxy)benzamido)-3-methylbutyl)(methyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1333239-53-4
C₃₇H₅₅N₃O₉

: 106-95-6
allyl bromide

: 1333239-59-0
tert-butyl ((2R,3R)-2-(allyloxy)-4-(N-((S)-1-((4-methoxybenzyl)-oxy)prop-2-yl)-5-nitro-2-(oct-7-en-1-yloxy)benzamido)-3-methylbutyl)(methyl)carbamate

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 - 25 ℃; for 12h; Inert atmosphere;
DOI:10.1021/jo2011957

Reference yield:

: 1333239-47-6
C₄₃H₆₉N₃O₉Si

: 1333239-59-0
tert-butyl ((2R,3R)-2-(allyloxy)-4-(N-((S)-1-((4-methoxybenzyl)-oxy)prop-2-yl)-5-nitro-2-(oct-7-en-1-yloxy)benzamido)-3-methylbutyl)(methyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 12.05 h / 0 - 25 °C / Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 12 h / 0 - 25 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jo2011957

Reference yield:

: 1333331-55-7
C₃₅H₅₄FN₃O₈Si

: 1333239-59-0
tert-butyl ((2R,3R)-2-(allyloxy)-4-(N-((S)-1-((4-methoxybenzyl)-oxy)prop-2-yl)-5-nitro-2-(oct-7-en-1-yloxy)benzamido)-3-methylbutyl)(methyl)carbamate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.33 h / 0 °C / Inert atmosphere

1.2: 2.03 h / 0 - 23 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 12.05 h / 0 - 25 °C / Inert atmosphere

3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 12 h / 0 - 25 °C / Inert atmosphere

With tetrabutyl ammonium fluoride; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jo2011957