N-(4-hydroxy-6-morpholino-1,3,5-triazin-2-yl)-4-methyl-N-(3-phenylprop-2-ynyl)benzenesulfonamide

Base Information

Chemical Name:N-(4-hydroxy-6-morpholino-1,3,5-triazin-2-yl)-4-methyl-N-(3-phenylprop-2-ynyl)benzenesulfonamide
CAS No.:1258620-77-7
Molecular Formula:C₂₃H₂₃N₅O₄S
Molecular Weight:465.533
Hs Code.:

Synonyms:N-(4-hydroxy-6-morpholino-1,3,5-triazin-2-yl)-4-methyl-N-(3-phenylprop-2-ynyl)benzenesulfonamide

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Chemical Property of N-(4-hydroxy-6-morpholino-1,3,5-triazin-2-yl)-4-methyl-N-(3-phenylprop-2-ynyl)benzenesulfonamide

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Technology Process of N-(4-hydroxy-6-morpholino-1,3,5-triazin-2-yl)-4-methyl-N-(3-phenylprop-2-ynyl)benzenesulfonamide

There total 4 articles about N-(4-hydroxy-6-morpholino-1,3,5-triazin-2-yl)-4-methyl-N-(3-phenylprop-2-ynyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 1258621-58-7
C₂₇H₃₂N₆O₄S

: 1258620-77-7
N-(4-hydroxy-6-morpholino-1,3,5-triazin-2-yl)-4-methyl-N-(3-phenylprop-2-ynyl)benzenesulfonamide

Guidance literature:: With copper(II) sulfate; sodium L-ascorbate; In water; acetonitrile; at 50 ℃;
DOI:10.1021/jo1016376

Reference yield:

: C₁₉H₁₄Cl₂N₄O₂S

: 1258620-77-7
N-(4-hydroxy-6-morpholino-1,3,5-triazin-2-yl)-4-methyl-N-(3-phenylprop-2-ynyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / acetonitrile / 0.5 h / 0 °C / Inert atmosphere

2: potassium tert-butylate / acetonitrile / 0.5 h / 0 °C / Inert atmosphere

3: copper(II) sulfate; sodium L-ascorbate / water; acetonitrile / 50 °C

With potassium tert-butylate; copper(II) sulfate; sodium L-ascorbate; N-ethyl-N,N-diisopropylamine; In water; acetonitrile;
DOI:10.1021/jo1016376

Reference yield:

: 1258620-73-3
N-(4-chloro-6-morpholino-1,3,5-triazin-2-yl)-4-methyl-N-(3-phenylprop-2-ynyl)benzenesulfonamide

: 1258620-77-7
N-(4-hydroxy-6-morpholino-1,3,5-triazin-2-yl)-4-methyl-N-(3-phenylprop-2-ynyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: potassium tert-butylate / acetonitrile / 0.5 h / 0 °C / Inert atmosphere

2: copper(II) sulfate; sodium L-ascorbate / water; acetonitrile / 50 °C

With potassium tert-butylate; copper(II) sulfate; sodium L-ascorbate; In water; acetonitrile;
DOI:10.1021/jo1016376