endo-2,3-diaza-10,10-diethoxy-1,4-diphenyltricyclo[5.2.1.0^5,9]dec-2-ene

Base Information

Chemical Name:endo-2,3-diaza-10,10-diethoxy-1,4-diphenyltricyclo[5.2.1.0^5,9]dec-2-ene
CAS No.:262420-94-0
Molecular Formula:C₂₄H₂₈N₂O₂
Molecular Weight:376.499
Hs Code.:

endo-2,3-diaza-10,10-diethoxy-1,4-diphenyltricyclo[5.2.1.0<sup>5,9</sup>]dec-2-ene

Synonyms:endo-2,3-diaza-10,10-diethoxy-1,4-diphenyltricyclo[5.2.1.0^5,9]dec-2-ene

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Chemical Property of endo-2,3-diaza-10,10-diethoxy-1,4-diphenyltricyclo[5.2.1.0^5,9]dec-2-ene

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Technology Process of endo-2,3-diaza-10,10-diethoxy-1,4-diphenyltricyclo[5.2.1.0^5,9]dec-2-ene

There total 4 articles about endo-2,3-diaza-10,10-diethoxy-1,4-diphenyltricyclo[5.2.1.0^5,9]dec-2-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 8,8-diethoxy-1,4-diphenyl-4,5,6,7-tetrahydro-1H-1,4-methano-cyclopenta[d]pyridazine

: 262420-94-0
endo-2,3-diaza-10,10-diethoxy-1,4-diphenyltricyclo[5.2.1.0^5,9]dec-2-ene

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; at 20 ℃; for 24h;
DOI:10.1021/ja992507j

Reference yield:

: 542-92-7,25568-84-7,7313-32-8
cyclopenta-1,3-diene

: 262420-94-0
endo-2,3-diaza-10,10-diethoxy-1,4-diphenyltricyclo[5.2.1.0^5,9]dec-2-ene

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / CH₂Cl₂ / 2 h / 20 °C

2: H₂ / Pd/C / ethyl acetate / 24 h / 20 °C

With hydrogen; trifluoroacetic acid; palladium on activated charcoal; In dichloromethane; ethyl acetate; 1: Addition / 2: Catalytic hydrogenation;
DOI:10.1021/ja992507j

Reference yield:

: 135127-41-2
4,4-Diethoxy-3,5-diphenyl-4H-pyrazol

: 262420-94-0
endo-2,3-diaza-10,10-diethoxy-1,4-diphenyltricyclo[5.2.1.0^5,9]dec-2-ene

Guidance literature:: Multi-step reaction with 2 steps

1: trifluoroacetic acid / CH₂Cl₂ / 2 h / 20 °C

2: H₂ / Pd/C / ethyl acetate / 24 h / 20 °C

With hydrogen; trifluoroacetic acid; palladium on activated charcoal; In dichloromethane; ethyl acetate; 1: Addition / 2: Catalytic hydrogenation;
DOI:10.1021/ja992507j