Technology Process of C66H85NO17
There total 4 articles about C66H85NO17 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: hydrazine hydrate / methanol; benzene / 6 h / 80 °C
2: methanol; CH2Cl2 / 4 h / 0 °C
With
hydrazine hydrate;
In
methanol; dichloromethane; benzene;
DOI:10.1021/ja00034a063
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 87 percent / AgOTf, HfCp2Cl2, 4 A molecular sieves / CH2Cl2 / 2 h / -40 - -10 °C
2: hydrazine hydrate / methanol; benzene / 6 h / 80 °C
3: methanol; CH2Cl2 / 4 h / 0 °C
With
bis(cyclopentadienyl)hafnium dichloride; 4 A molecular sieve; silver trifluoromethanesulfonate; hydrazine hydrate;
In
methanol; dichloromethane; benzene;
DOI:10.1021/ja00034a063
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 87 percent / AgOTf, HfCp2Cl2, 4 A molecular sieves / CH2Cl2 / 2 h / -40 - -10 °C
2: hydrazine hydrate / methanol; benzene / 6 h / 80 °C
3: methanol; CH2Cl2 / 4 h / 0 °C
With
bis(cyclopentadienyl)hafnium dichloride; 4 A molecular sieve; silver trifluoromethanesulfonate; hydrazine hydrate;
In
methanol; dichloromethane; benzene;
DOI:10.1021/ja00034a063