Technology Process of C17H15BrN2
There total 4 articles about C17H15BrN2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-Bromosuccinimide;
In
acetonitrile;
at 0 - 20 ℃;
for 1.16667h;
DOI:10.1021/ja311682c
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium iodide; sulfuric acid / 1.05 h / 0 - 140 °C / Schlenk technique
2: 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate; sodium tert-pentoxide / toluene / 24 h / 120 °C / Glovebox; Inert atmosphere
3: N-Bromosuccinimide / acetonitrile / 1.17 h / 0 - 20 °C
With
N-Bromosuccinimide; sulfuric acid; palladium diacetate; sodium tert-pentoxide; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium iodide;
In
toluene; acetonitrile;
DOI:10.1021/ja311682c
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-Bromosuccinimide / acetonitrile / 3.5 h / 0 - 20 °C
2: sodium iodide; sulfuric acid / 1.05 h / 0 - 140 °C / Schlenk technique
3: 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; palladium diacetate; sodium tert-pentoxide / toluene / 24 h / 120 °C / Glovebox; Inert atmosphere
4: N-Bromosuccinimide / acetonitrile / 1.17 h / 0 - 20 °C
With
N-Bromosuccinimide; sulfuric acid; palladium diacetate; sodium tert-pentoxide; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium iodide;
In
toluene; acetonitrile;
DOI:10.1021/ja311682c