3-(4-benzyloxy-3-bromo-phenyl)-5,7-dichloro-3-methyl-1H-quinoline-2,4-dione

Base Information

• Chemical Name: 3-(4-benzyloxy-3-bromo-phenyl)-5,7-dichloro-3-methyl-1H-quinoline-2,4-dione
• CAS No.: 883243-89-8
• Molecular Formula: C₂₃H₁₆BrCl₂NO₃
• Molecular Weight: 505.195

Synonyms:3-(4-benzyloxy-3-bromo-phenyl)-5,7-dichloro-3-methyl-1H-quinoline-2,4-dione

Chemical Property of 3-(4-benzyloxy-3-bromo-phenyl)-5,7-dichloro-3-methyl-1H-quinoline-2,4-dione

Chemical Property:

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Technology Process of 3-(4-benzyloxy-3-bromo-phenyl)-5,7-dichloro-3-methyl-1H-quinoline-2,4-dione

There total 2 articles about 3-(4-benzyloxy-3-bromo-phenyl)-5,7-dichloro-3-methyl-1H-quinoline-2,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

2-[2-(4-benzyloxy-3-bromo-phenyl)-propionylamino]-4,6-dichloro-benzoic acid methyl ester (883244-30-2) → 3-(4-benzyloxy-3-bromo-phenyl)-5,7-dichloro-3-methyl-1H-quinoline-2,4-dione (883243-89-8)

Guidance literature:

With lithium hexamethyldisilazane; In tetrahydrofuran; hexane; Heating;

DOI:10.1016/j.bmcl.2007.11.045

Reference yield: 67.0%

→ 3-(4-benzyloxy-3-bromo-phenyl)-5,7-dichloro-3-methyl-1H-quinoline-2,4-dione (883243-89-8)

Guidance literature:

Reference yield: 78.0%

3-(4-benzyloxy-3-bromo-phenyl)-5,7-dichloro-3-methyl-1H-quinoline-2,4-dione (883243-89-8) → 3-(3-bromo-4-hydroxy-phenyl)-5,7-dichloro-3-methyl-1H-quinoline-2,4-dione

Guidance literature:

With boron tribromide; In dichloromethane; at 20 ℃; for 12h;

DOI:10.1016/j.bmcl.2007.11.045

upstream raw materials:

2-[2-(4-benzyloxy-3-bromo-phenyl)-propionylamino]-4,6-dichloro-benzoic acid methyl ester

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