chloro-2S (dichloro-2,6 benzyloxy)-3R butyrate de methyle

Base Information

Chemical Name:chloro-2S (dichloro-2,6 benzyloxy)-3R butyrate de methyle
CAS No.:103548-52-3
Molecular Formula:C₁₂H₁₃Cl₃O₃
Molecular Weight:311.592
Hs Code.:

Synonyms:chloro-2S (dichloro-2,6 benzyloxy)-3R butyrate de methyle

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Chemical Property of chloro-2S (dichloro-2,6 benzyloxy)-3R butyrate de methyle

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Technology Process of chloro-2S (dichloro-2,6 benzyloxy)-3R butyrate de methyle

There total 4 articles about chloro-2S (dichloro-2,6 benzyloxy)-3R butyrate de methyle which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1035797-94-4
trichloroacetamidate de dichloro-2,6 benzyle

: 103618-21-9
chloro-2R hydroxy-3S butyrate de methyle

: 103548-52-3
chloro-2R (dichloro-2,6 benzyloxy)-3S butyrate de methyle

Guidance literature:: With trifluorormethanesulfonic acid; In dichloromethane; cyclohexane; for 40h; Ambient temperature;
DOI:10.1016/S0040-4020(01)96784-5

Reference yield:

: 103618-23-1
chloro-2S hydroxy-3R butyrate de methyle

: 1035797-94-4
trichloroacetamidate de dichloro-2,6 benzyle

: 103548-52-3
chloro-2S (dichloro-2,6 benzyloxy)-3R butyrate de methyle

Guidance literature:: With trifluorormethanesulfonic acid; In dichloromethane; cyclohexane; for 40h; Ambient temperature;
DOI:10.1016/S0040-4020(01)96784-5

Reference yield:

: 15258-73-8
2,6-dichlorobenzyl alcohol

: 103548-52-3
chloro-2S (dichloro-2,6 benzyloxy)-3R butyrate de methyle

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium metallique / 1.) benzene, 1 h; 2.) benzene, 6 h, RT

2: d'acide trfluoromethanesulfonique / cyclohexane; CH₂Cl₂ / 40 h / Ambient temperature

With trifluorormethanesulfonic acid; sodium; In dichloromethane; cyclohexane;
DOI:10.1016/S0040-4020(01)96784-5