N_ε-<6-hexanoyl>-N_α-(tert-butyloxycarbonyl)-L-lysine

Base Information

Chemical Name:N_ε-<6-hexanoyl>-N_α-(tert-butyloxycarbonyl)-L-lysine
CAS No.:224577-24-6
Molecular Formula:C₂₅H₃₉N₃O₇
Molecular Weight:493.601
Hs Code.:

N<sub>ε</sub>-<6-<N-(benzyloxycarbonyl)amino>hexanoyl>-N<sub>α</sub>-(tert-butyloxycarbonyl)-L-lysine

Synonyms:N_ε-<6-hexanoyl>-N_α-(tert-butyloxycarbonyl)-L-lysine

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Chemical Property of N_ε-<6-hexanoyl>-N_α-(tert-butyloxycarbonyl)-L-lysine

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Technology Process of N_ε-<6-hexanoyl>-N_α-(tert-butyloxycarbonyl)-L-lysine

There total 4 articles about N_ε-<6-hexanoyl>-N_α-(tert-butyloxycarbonyl)-L-lysine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 224577-23-5
N_ε-<6-hexanoyl>-N_α-(tert-butyloxycarbonyl)-L-lysine methyl ester

: 224577-24-6
N_ε-<6-hexanoyl>-N_α-(tert-butyloxycarbonyl)-L-lysine

Guidance literature:: With lithium hydroxide; In methanol; for 16h; Ambient temperature;
DOI:10.1021/jm980673g

Reference yield:

: 1947-00-8
6-(benzyloxycarbonylamino)hexanoic acid

: 224577-24-6
N_ε-<6-hexanoyl>-N_α-(tert-butyloxycarbonyl)-L-lysine

Guidance literature:: Multi-step reaction with 2 steps

1: 58 percent / HOBt, Et₃N, EDC / dimethylformamide / 2 h

2: 92 percent / 2 N LiOH / methanol / 16 h / Ambient temperature

With lithium hydroxide; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm980673g

Reference yield:

: 501-53-1,94274-21-2
benzyl chloroformate

: 224577-24-6
N_ε-<6-hexanoyl>-N_α-(tert-butyloxycarbonyl)-L-lysine

Guidance literature:: Multi-step reaction with 3 steps

1: 32 percent / Na₂CO₃, 2 N aq. NaOH / 1 h / 0 - 20 °C

2: 58 percent / HOBt, Et₃N, EDC / dimethylformamide / 2 h

3: 92 percent / 2 N LiOH / methanol / 16 h / Ambient temperature

With lithium hydroxide; sodium hydroxide; sodium carbonate; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm980673g