<2-<1',1'-bis(ethoxycarbonyl)-4'-oxopentyl>cyclobutyl>triphenylphosphonium perchlorate

Base Information

Chemical Name:<2-<1',1'-bis(ethoxycarbonyl)-4'-oxopentyl>cyclobutyl>triphenylphosphonium perchlorate
CAS No.:118418-40-9
Molecular Formula:C₃₃H₃₈O₅P*ClO₄
Molecular Weight:645.086
Hs Code.:

Synonyms:<2-<1',1'-bis(ethoxycarbonyl)-4'-oxopentyl>cyclobutyl>triphenylphosphonium perchlorate

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Chemical Property of <2-<1',1'-bis(ethoxycarbonyl)-4'-oxopentyl>cyclobutyl>triphenylphosphonium perchlorate

Chemical Property:

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Technology Process of <2-<1',1'-bis(ethoxycarbonyl)-4'-oxopentyl>cyclobutyl>triphenylphosphonium perchlorate

There total 4 articles about <2-<1',1'-bis(ethoxycarbonyl)-4'-oxopentyl>cyclobutyl>triphenylphosphonium perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: {2-[1,1-Bis-ethoxycarbonyl-3-(2-methyl-[1,3]dioxolan-2-yl)-propyl]-cyclobutyl}-triphenyl-phosphonium; perchlorate

: 118418-40-9
<2-<1',1'-bis(ethoxycarbonyl)-4'-oxopentyl>cyclobutyl>triphenylphosphonium perchlorate

Guidance literature:: With perchloric acid; for 1h; Heating;
DOI:10.1021/jo00265a047

Reference yield: 62.0%

: 4761-26-6
ethyl 2-carbethoxy-5-oxocaproate

: 86046-73-3
(1-cyclobutenyl)triphenylphosphonium perchlorate

: 118418-40-9
<2-<1',1'-bis(ethoxycarbonyl)-4'-oxopentyl>cyclobutyl>triphenylphosphonium perchlorate

Guidance literature:: With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; 1.) RT, overnight, 2.) reflux, 1 h;
DOI:10.1021/jo00265a047

Reference yield:

: 7796-23-8
(3-oxybutyl)malonate ethylene ketal

: 118418-40-9
<2-<1',1'-bis(ethoxycarbonyl)-4'-oxopentyl>cyclobutyl>triphenylphosphonium perchlorate

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / NaH / tetrahydrofuran; dimethylformamide / Ambient temperature

2: 100 percent / hydroperchloric acid / 1 h / Heating

With perchloric acid; sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo00265a047