1-(dimethylphenylsilyl)-3,3-dimethyl-2-butyl trifluoroacetate

Base Information

Chemical Name:1-(dimethylphenylsilyl)-3,3-dimethyl-2-butyl trifluoroacetate
CAS No.:1252913-80-6
Molecular Formula:C₁₆H₂₃F₃O₂Si
Molecular Weight:332.438
Hs Code.:

Synonyms:1-(dimethylphenylsilyl)-3,3-dimethyl-2-butyl trifluoroacetate

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Chemical Property of 1-(dimethylphenylsilyl)-3,3-dimethyl-2-butyl trifluoroacetate

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Technology Process of 1-(dimethylphenylsilyl)-3,3-dimethyl-2-butyl trifluoroacetate

There total 3 articles about 1-(dimethylphenylsilyl)-3,3-dimethyl-2-butyl trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1252913-97-5
1-(dimethylphenylsilyl)-3,3-dimethyl-2-butanol

: 407-25-0
trifluoroacetic anhydride

: 1252913-80-6
1-(dimethylphenylsilyl)-3,3-dimethyl-2-butyl trifluoroacetate

Guidance literature:: With pyridine; In diethyl ether; at 0 ℃; for 2h;
DOI:10.1002/poc.1667

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 1252913-80-6
1-(dimethylphenylsilyl)-3,3-dimethyl-2-butyl trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

2.1: magnesium / diethyl ether

2.2: 3 h / 0 - 20 °C

3.1: pyridine / diethyl ether / 2 h / 0 °C

With pyridine; magnesium; In diethyl ether; 1.1: Grignard reaction / 2.2: Grignard reaction;
DOI:10.1002/poc.1667

Reference yield:

: 1833-51-8
chloromethyldimethylphenylsilane

: 1252913-80-6
1-(dimethylphenylsilyl)-3,3-dimethyl-2-butyl trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: magnesium / diethyl ether

1.2: 3 h / 0 - 20 °C

2.1: pyridine / diethyl ether / 2 h / 0 °C

With pyridine; magnesium; In diethyl ether; 1.2: Grignard reaction;
DOI:10.1002/poc.1667