N-(1-pyridinio)-p-toluamidate

Base Information

• Chemical Name: N-(1-pyridinio)-p-toluamidate
• CAS No.: 36048-78-9
• Molecular Formula: C₁₃H₁₂N₂O
• Molecular Weight: 212.251

Synonyms:N-(1-pyridinio)-p-toluamidate

Chemical Property of N-(1-pyridinio)-p-toluamidate

Chemical Property:

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Technology Process of N-(1-pyridinio)-p-toluamidate

There total 2 articles about N-(1-pyridinio)-p-toluamidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

N-aminopyridin-1-ium iodide (6295-87-0) + 4-methyl-benzoyl chloride (874-60-2) → N-(1-pyridinio)-p-toluamidate (36048-78-9)

Guidance literature:

With sodium hydroxide; at 25 ℃; for 24h;

DOI:10.1021/jm00348a021

Reference yield:

→ N-(1-pyridinio)-p-toluamidate (36048-78-9)

Guidance literature:

1-Aminopyridiniumiodid, p-Tolylchlorid;

DOI:10.1186/BF03351660

Reference yield: 98.0%

N-(1-pyridinio)-p-toluamidate (36048-78-9) → N-(3,6-Dihydro-2H-pyridin-1-yl)-4-methyl-benzamide (81460-52-8)

Guidance literature:

With sodium tetrahydroborate; In ethanol; at 0 ℃; for 5h;

DOI:10.1021/jm00348a021

upstream raw materials:

N-aminopyridin-1-ium iodide

4-methyl-benzoyl chloride

Downstream raw materials:

4,5-diphenyl-2-p-tolyl-[1,3]oxazine-6-thione

N-(3,6-Dihydro-2H-pyridin-1-yl)-4-methyl-benzamide

6-methyl-3,4-diphenylisoquinolin-1(2H)-one

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