3-<(4-Methoxyphenyl)methyl>-3H-1,2,3-triazolo<4,5-b><1,5>benzoxazepin-10(9H)-one

Base Information

Chemical Name:3-<(4-Methoxyphenyl)methyl>-3H-1,2,3-triazolo<4,5-b><1,5>benzoxazepin-10(9H)-one
CAS No.:106157-45-3
Molecular Formula:C₁₇H₁₄N₄O₃
Molecular Weight:322.323
Hs Code.:

Synonyms:3-<(4-Methoxyphenyl)methyl>-3H-1,2,3-triazolo<4,5-b><1,5>benzoxazepin-10(9H)-one

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Chemical Property of 3-<(4-Methoxyphenyl)methyl>-3H-1,2,3-triazolo<4,5-b><1,5>benzoxazepin-10(9H)-one

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Technology Process of 3-<(4-Methoxyphenyl)methyl>-3H-1,2,3-triazolo<4,5-b><1,5>benzoxazepin-10(9H)-one

There total 3 articles about 3-<(4-Methoxyphenyl)methyl>-3H-1,2,3-triazolo<4,5-b><1,5>benzoxazepin-10(9H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 106157-40-8
5-Chloro-1-(4-methoxy-benzyl)-1H-[1,2,3]triazole-4-carboxylic acid (2-hydroxy-phenyl)-amide

: 106157-45-3
3-<(4-Methoxyphenyl)methyl>-3H-1,2,3-triazolo<4,5-b><1,5>benzoxazepin-10(9H)-one

Guidance literature:: With potassium tert-butylate; In dimethyl sulfoxide; at 80 ℃; for 42h;
DOI:10.1002/jhet.5570220645

Reference yield:

: 96938-91-9
5-Chloro-1-<(4-methoxyphenyl)methyl>-1H-1,2,3-triazole-4-carbonyl chloride

: 106157-45-3
3-<(4-Methoxyphenyl)methyl>-3H-1,2,3-triazolo<4,5-b><1,5>benzoxazepin-10(9H)-one

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / ethyl acetate / 3 h / Ambient temperature

2: 49 percent / potassium t-butoxide / dimethylsulfoxide / 42 h / 80 °C

With potassium tert-butylate; In dimethyl sulfoxide; ethyl acetate;
DOI:10.1002/jhet.5570220645

Reference yield:

: 97326-40-4
5-Hydroxy-1-<(4-methoxyphenyl)methyl>-1H-1,2,3-triazolo-4-carboxylic Acid

: 106157-45-3
3-<(4-Methoxyphenyl)methyl>-3H-1,2,3-triazolo<4,5-b><1,5>benzoxazepin-10(9H)-one

Guidance literature:: Multi-step reaction with 3 steps

1: 52 percent / PCl₅ / toluene / 1) 40 deg C, 7h; 2) reflux, 4h

2: 91 percent / ethyl acetate / 3 h / Ambient temperature

3: 49 percent / potassium t-butoxide / dimethylsulfoxide / 42 h / 80 °C

With phosphorus pentachloride; potassium tert-butylate; In dimethyl sulfoxide; ethyl acetate; toluene;
DOI:10.1002/jhet.5570220645