Technology Process of C15H24N2O2
There total 6 articles about C15H24N2O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
10% palladium on activated carbon; hydrogen;
In
methanol;
for 1h;
under 2327.23 Torr;
DOI:10.1016/j.tetlet.2011.04.049
- Guidance literature:
-
Multi-step reaction with 3 steps
1: lithium borohydride / tetrahydrofuran / 1 h / 0 - 20 °C
2: triethylamine / dichloromethane / 6 h / 0 - 20 °C
3: 10% palladium on activated carbon; hydrogen / methanol / 1 h / 2327.23 Torr
With
lithium borohydride; 10% palladium on activated carbon; hydrogen; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.tetlet.2011.04.049
- Guidance literature:
-
Multi-step reaction with 4 steps
1: thionyl chloride / 0 °C
2: lithium borohydride / tetrahydrofuran / 1 h / 0 - 20 °C
3: triethylamine / dichloromethane / 6 h / 0 - 20 °C
4: 10% palladium on activated carbon; hydrogen / methanol / 1 h / 2327.23 Torr
With
lithium borohydride; thionyl chloride; 10% palladium on activated carbon; hydrogen; triethylamine;
In
tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.tetlet.2011.04.049