C₂₂H₂₁N₃O₂

Base Information

Chemical Name:C₂₂H₂₁N₃O₂
CAS No.:1323444-34-3
Molecular Formula:C₂₂H₂₁N₃O₂
Molecular Weight:359.428
Hs Code.:

C<sub>22</sub>H<sub>21</sub>N<sub>3</sub>O<sub>2</sub>

Synonyms:C₂₂H₂₁N₃O₂

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Chemical Property of C₂₂H₂₁N₃O₂

Chemical Property:

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Technology Process of C₂₂H₂₁N₃O₂

There total 6 articles about C₂₂H₂₁N₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 1323444-33-2
C₂₂H₂₀N₂O₂

: 1323444-34-3
C₂₂H₂₁N₃O₂

Guidance literature:: With hydroxylamine hydrochloride; sodium acetate; In methanol; for 5h; Reflux;
DOI:10.1016/j.bmcl.2011.05.052

Reference yield:

: 150159-15-2
C₁₅H₁₄N₂O₂

: 1323444-34-3
C₂₂H₂₁N₃O₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

1.2: 20 °C

2.1: hydroxylamine hydrochloride; sodium acetate / methanol / 5 h / Reflux

With hydroxylamine hydrochloride; sodium acetate; sodium hydride; In methanol; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.05.052

Reference yield:

: 35302-72-8
pyrrol-2-yl trichloromethyl ketone

: 1323444-34-3
C₂₂H₂₁N₃O₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: triethylamine / acetonitrile / 20 °C

2.1: sodium hydroxide

2.2: 20 °C

3.1: phosphorus pentoxide

4.1: potassium carbonate / acetonitrile / 8 h / Reflux

5.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

5.2: 20 °C

6.1: hydroxylamine hydrochloride; sodium acetate / methanol / 5 h / Reflux

With phosphorus pentoxide; hydroxylamine hydrochloride; sodium acetate; sodium hydride; potassium carbonate; triethylamine; sodium hydroxide; In methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmcl.2011.05.052