N,N'-bis<6-<2-hydroxy-2-(3,4,5-trimethoxyphenyl)ethylamino>hexyl>cystamine

Base Information

Chemical Name:N,N'-bis<6-<2-hydroxy-2-(3,4,5-trimethoxyphenyl)ethylamino>hexyl>cystamine
CAS No.:102104-82-5
Molecular Formula:C₃₈H₆₆N₄O₈S₂
Molecular Weight:771.096
Hs Code.:

Synonyms:N,N'-bis<6-<2-hydroxy-2-(3,4,5-trimethoxyphenyl)ethylamino>hexyl>cystamine

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Chemical Property of N,N'-bis<6-<2-hydroxy-2-(3,4,5-trimethoxyphenyl)ethylamino>hexyl>cystamine

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Technology Process of N,N'-bis<6-<2-hydroxy-2-(3,4,5-trimethoxyphenyl)ethylamino>hexyl>cystamine

There total 3 articles about N,N'-bis<6-<2-hydroxy-2-(3,4,5-trimethoxyphenyl)ethylamino>hexyl>cystamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 102104-68-7
3-<6-<2-hydroxy-2-(3,4,5-trimethoxyphenyl)ethylamino>hexyl>-1,3-thiazolidine

: 102104-82-5
N,N'-bis<6-<2-hydroxy-2-(3,4,5-trimethoxyphenyl)ethylamino>hexyl>cystamine

Guidance literature:: With hydrogenchloride; iodine; potassium iodide; In ethanol; for 12h; Ambient temperature;
DOI:10.1002/jhet.5570220326

Reference yield:

: 88346-63-8
3-(6-aminohexyl)-1,3-thiazolidine

: 102104-82-5
N,N'-bis<6-<2-hydroxy-2-(3,4,5-trimethoxyphenyl)ethylamino>hexyl>cystamine

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / propan-2-ol / 22 h / Heating

2: 89 percent / aq. I₂/KI, aq. HCl / ethanol / 12 h / 25 °C

With hydrogenchloride; iodine; potassium iodide; In ethanol; isopropyl alcohol;
DOI:10.1021/jm00390a011

Reference yield:

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 102104-82-5
N,N'-bis<6-<2-hydroxy-2-(3,4,5-trimethoxyphenyl)ethylamino>hexyl>cystamine

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / aq. sodium hydroxide (50 percent), tetrabuthylammonium bromide / CH₂Cl₂ / 96 h / 50 °C

2: 77 percent / propan-2-ol / 22 h / Heating

3: 89 percent / iodine (0.1 N)-potassium iodide (2.5 percent), hydrochloric acid (2N) / ethanol / 12 h / Ambient temperature

With hydrogenchloride; sodium hydroxide; tetrabutylammomium bromide; iodine; potassium iodide; In ethanol; dichloromethane; isopropyl alcohol;
DOI:10.1002/jhet.5570220326