Technology Process of C46H47N3O9
There total 3 articles about C46H47N3O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
lithium hydroxide;
In
tetrahydrofuran; water;
at 40 ℃;
Microwave irradiation;
DOI:10.1016/j.bmcl.2010.12.126
- Guidance literature:
-
Multi-step reaction with 2 steps
1: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; N,N-dimethyl-formamide / 60 °C / Microwave irradiation
2: lithium hydroxide / tetrahydrofuran; water / 40 °C / Microwave irradiation
With
copper(ll) sulfate pentahydrate; sodium L-ascorbate; lithium hydroxide;
In
tetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2010.12.126
- Guidance literature:
-
Multi-step reaction with 3 steps
1: imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; potassium carbonate / methanol; water / 6 h / 20 °C
2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; N,N-dimethyl-formamide / 60 °C / Microwave irradiation
3: lithium hydroxide / tetrahydrofuran; water / 40 °C / Microwave irradiation
With
imidazole-1-sulfonyl azide hydrochloride; copper(ll) sulfate pentahydrate; potassium carbonate; sodium L-ascorbate; lithium hydroxide;
In
tetrahydrofuran; methanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2010.12.126