N-(3,4-dimethoxyphenetyl)-2-(2-naphthyl)-m-dithiane-2-propanamine hydrochloride

Base Information

Chemical Name:N-(3,4-dimethoxyphenetyl)-2-(2-naphthyl)-m-dithiane-2-propanamine hydrochloride
CAS No.:127772-58-1
Molecular Formula:C₂₇H₃₃NO₂S₂*ClH
Molecular Weight:504.157
Hs Code.:

Synonyms:N-(3,4-dimethoxyphenetyl)-2-(2-naphthyl)-m-dithiane-2-propanamine hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3,4-dimethoxyphenetyl)-2-(2-naphthyl)-m-dithiane-2-propanamine hydrochloride

Chemical Property:

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Technology Process of N-(3,4-dimethoxyphenetyl)-2-(2-naphthyl)-m-dithiane-2-propanamine hydrochloride

There total 7 articles about N-(3,4-dimethoxyphenetyl)-2-(2-naphthyl)-m-dithiane-2-propanamine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21473-01-8
2-naphthalenylmagnesium bromide

: 127772-58-1
N-(3,4-dimethoxyphenetyl)-2-(2-naphthyl)-m-dithiane-2-propanamine hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

2: 97 percent / anhydrous SnCl₂ / tetrahydrofuran

3: 79 percent / n-BuLi / hexane; tetrahydrofuran

4: 1.) sodium borohydride; 2.) HCl/dioxane / ethanol / 64 h / Ambient temperature

With hydrogenchloride; sodium tetrahydroborate; n-butyllithium; tin(ll) chloride; In tetrahydrofuran; ethanol; hexane;
DOI:10.1016/0223-5234(89)90053-6

Reference yield:

: 127772-51-4
N-(3,4-dimethoxyphenetyl)-2,2,2-trifluoro-N-<3-<2-(2-naphthyl)-m-dithian-2-yl>-propyl->acetamide

: 127772-58-1
N-(3,4-dimethoxyphenetyl)-2-(2-naphthyl)-m-dithiane-2-propanamine hydrochloride

Guidance literature:: With hydrogenchloride; sodium tetrahydroborate; In ethanol; for 64h; Ambient temperature;
DOI:10.1016/0223-5234(89)90053-6

Reference yield:

: 13230-71-2
N-[2-(3,4-dimethoxyphenyl)ethyl]-2,2,2-trifluoroacetamide

: 127772-58-1
N-(3,4-dimethoxyphenetyl)-2-(2-naphthyl)-m-dithiane-2-propanamine hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 56 percent / KOH / acetone / 2 h / Heating

2: 79 percent / n-BuLi / hexane; tetrahydrofuran

3: 1.) sodium borohydride; 2.) HCl/dioxane / ethanol / 64 h / Ambient temperature

With hydrogenchloride; potassium hydroxide; sodium tetrahydroborate; n-butyllithium; In tetrahydrofuran; ethanol; hexane; acetone;
DOI:10.1016/0223-5234(89)90053-6