p-methylphenyl 2-O-acetyl-3-O-benzoyl-6-deoxy-6-iodo-1-thio-β-D-galactopyranoside

Base Information

Chemical Name:p-methylphenyl 2-O-acetyl-3-O-benzoyl-6-deoxy-6-iodo-1-thio-β-D-galactopyranoside
CAS No.:1042430-55-6
Molecular Formula:C₂₂H₂₃IO₆S
Molecular Weight:542.392
Hs Code.:

Synonyms:p-methylphenyl 2-O-acetyl-3-O-benzoyl-6-deoxy-6-iodo-1-thio-β-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-methylphenyl 2-O-acetyl-3-O-benzoyl-6-deoxy-6-iodo-1-thio-β-D-galactopyranoside

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Technology Process of p-methylphenyl 2-O-acetyl-3-O-benzoyl-6-deoxy-6-iodo-1-thio-β-D-galactopyranoside

There total 2 articles about p-methylphenyl 2-O-acetyl-3-O-benzoyl-6-deoxy-6-iodo-1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1042430-54-5
p-methylphenyl 2-O-acetyl-3-O-benzoyl-1-thio-β-D-galactopyranoside

: 1042430-55-6
p-methylphenyl 2-O-acetyl-3-O-benzoyl-6-deoxy-6-iodo-1-thio-β-D-galactopyranoside

Guidance literature:: With N-iodosaccharine; triphenylphosphine; In dichloromethane; for 20h; Heating;
DOI:10.1016/j.carres.2007.11.030

Reference yield:

: 1206451-67-3
p-methylphenyl 2-O-acetyl-3-O-benzoyl-4-O-benzyl-6-deoxy-6-iodo-1-thio-β-D-galactopyranoside

: 1042430-55-6
p-methylphenyl 2-O-acetyl-3-O-benzoyl-6-deoxy-6-iodo-1-thio-β-D-galactopyranoside

Guidance literature:: With palladium on carbon; hydrogen; sodium hydrogencarbonate; In N,N-dimethyl-formamide; for 5h; under 760.051 Torr;
DOI:10.1039/b914534f

Reference yield: 76.0%

: 1042430-55-6
p-methylphenyl 2-O-acetyl-3-O-benzoyl-6-deoxy-6-iodo-1-thio-β-D-galactopyranoside

: 1042430-56-7
p-methylphenyl 2-O-acetyl-3-O-benzoyl-1-thio-β-D-fucopyranoside

Guidance literature:: With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In N,N-dimethyl-formamide; for 12h; under 18751.9 Torr;
DOI:10.1016/j.carres.2007.11.030