Technology Process of C32H38O5Si
There total 12 articles about C32H38O5Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
5% Pd-BaSO4; hydrogen;
In
ethyl acetate;
at 20 ℃;
for 12h;
under 750.075 Torr;
DOI:10.1002/chem.201102192
- Guidance literature:
-
Multi-step reaction with 7 steps
1: triethylamine / tetrahydrofuran / 0 - 20 °C
2: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 96 h / 20 °C
3: tetrahydrofuran / 4 h / Reflux
4: 5% Pd-BaSO4; hydrogen / ethyl acetate / 0.67 h / 20 °C / 750.08 Torr
5: toluene-4-sulfonic acid / tetrahydrofuran / 72 h / 20 °C
6: toluene-4-sulfonic acid / benzene / 16 h / Reflux
7: 5% Pd-BaSO4; hydrogen / ethyl acetate / 12 h / 20 °C / 750.08 Torr
With
osmium(VIII) oxide; 5% Pd-BaSO4; hydrogen; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; triethylamine;
In
tetrahydrofuran; water; ethyl acetate; acetone; benzene;
DOI:10.1002/chem.201102192
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 5% Pd-BaSO4; hydrogen / ethyl acetate / 0.67 h / 20 °C / 750.08 Torr
2: toluene-4-sulfonic acid / tetrahydrofuran / 72 h / 20 °C
3: toluene-4-sulfonic acid / benzene / 16 h / Reflux
4: 5% Pd-BaSO4; hydrogen / ethyl acetate / 12 h / 20 °C / 750.08 Torr
With
5% Pd-BaSO4; hydrogen; toluene-4-sulfonic acid;
In
tetrahydrofuran; ethyl acetate; benzene;
DOI:10.1002/chem.201102192
