2,3-Bis(3,5-dichloro-2-(phenylthio)phenyl)propylamine

Base Information

Chemical Name:2,3-Bis(3,5-dichloro-2-(phenylthio)phenyl)propylamine
CAS No.:79332-40-4
Molecular Formula:C₂₇H₂₁Cl₄NS₂
Molecular Weight:565.414
Hs Code.:
DSSTox Substance ID:DTXSID201000403
Mol file:79332-40-4.mol

Synonyms:BRN 4728133;79332-40-4;2,3-Bis(3,5-dichloro-2-(phenylthio)phenyl)propylamine;Benzenepropanamine, 3,5-dichloro-beta-(3,5-dichloro-2-(phenylthio)phenyl)-2-(phenylthio)-;C27H21Cl4NS2;DTXSID201000403;C27-H21-Cl4-N-S2;LS-31031;2,3-Bis[3,5-dichloro-2-(phenylsulfanyl)phenyl]propan-1-amine

Suppliers and Price of 2,3-Bis(3,5-dichloro-2-(phenylthio)phenyl)propylamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2,3-BIS(3,5-DICHLORO-2-(PHENYLTHIO)PHENYL)PROPYLAMINE 95.00%
5MG
$ 500.91

Total 4 raw suppliers

Chemical Property of 2,3-Bis(3,5-dichloro-2-(phenylthio)phenyl)propylamine

Chemical Property:

Vapor Pressure:8.32E-14mmHg at 25°C
Refractive Index:1.712
Boiling Point:588°C at 760 mmHg
Flash Point:309.4°C
PSA：76.62000
Density:1.44g/cm³
LogP:10.58790
XLogP3:9.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:8
Exact Mass:564.984003
Heavy Atom Count:34
Complexity:601

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

2,3-BIS(3,5-DICHLORO-2-(PHENYLTHIO)PHENYL)PROPYLAMINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)SC2=C(C=C(C=C2Cl)Cl)CC(CN)C3=C(C(=CC(=C3)Cl)Cl)SC4=CC=CC=C4

Technology Process of 2,3-Bis(3,5-dichloro-2-(phenylthio)phenyl)propylamine

There total 6 articles about 2,3-Bis(3,5-dichloro-2-(phenylthio)phenyl)propylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15396-37-9
2-iodoyl-3,5-dichlorobenzoic acid

: 79332-40-4
2,3-bis<3,5-dichloro-2-(phenylthio)phenyl>propylamine

Guidance literature:: Multi-step reaction with 5 steps

1: 78 percent / K₂CO₃, CuCl / dimethylformamide / 4 h / 140 °C

2: 87 percent / LiAlH₄ / diethyl ether / 2.5 h / Heating

3: 96 percent / SOCl₂ / benzene / 1.) 25 deg C, 20 min 2.) 60 deg C, 1 h 3.) reflux 1.5 h

4: KI / acetone / 5 h / Heating

5: LiAlH₄ / diethyl ether / 2.5 h / Heating

With lithium aluminium tetrahydride; thionyl chloride; potassium carbonate; copper(l) chloride; potassium iodide; In diethyl ether; N,N-dimethyl-formamide; acetone; benzene;
DOI:10.1135/cccc19810781

Reference yield:

: 79332-30-2
3,5-dichloro-2-(phenylthio)benzoic acid

: 79332-40-4
2,3-bis<3,5-dichloro-2-(phenylthio)phenyl>propylamine

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / LiAlH₄ / diethyl ether / 2.5 h / Heating

2: 96 percent / SOCl₂ / benzene / 1.) 25 deg C, 20 min 2.) 60 deg C, 1 h 3.) reflux 1.5 h

3: KI / acetone / 5 h / Heating

4: LiAlH₄ / diethyl ether / 2.5 h / Heating

With lithium aluminium tetrahydride; thionyl chloride; potassium iodide; In diethyl ether; acetone; benzene;
DOI:10.1135/cccc19810781

Reference yield:

: 79332-32-4
3,5-dichloro-2-(phenylthio)benzyl alcohol

: 79332-40-4
2,3-bis<3,5-dichloro-2-(phenylthio)phenyl>propylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / SOCl₂ / benzene / 1.) 25 deg C, 20 min 2.) 60 deg C, 1 h 3.) reflux 1.5 h

2: KI / acetone / 5 h / Heating

3: LiAlH₄ / diethyl ether / 2.5 h / Heating

With lithium aluminium tetrahydride; thionyl chloride; potassium iodide; In diethyl ether; acetone; benzene;
DOI:10.1135/cccc19810781