ethyl p-acetonyl>amino>benzoate hydrochloride

Base Information

Chemical Name:ethyl p-acetonyl>amino>benzoate hydrochloride
CAS No.:101760-54-7
Molecular Formula:C₁₉H₂₀N₆O₆*ClH
Molecular Weight:464.865
Hs Code.:

ethyl p-<N-propargyl-N-<3-<(2-amino-4-hydroxy-5-nitropyrimidin-6-yl)amino>acetonyl>amino>benzoate hydrochloride

Synonyms:ethyl p-acetonyl>amino>benzoate hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl p-acetonyl>amino>benzoate hydrochloride

Chemical Property:

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Technology Process of ethyl p-acetonyl>amino>benzoate hydrochloride

There total 3 articles about ethyl p-acetonyl>amino>benzoate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 101760-52-5
ethyl p-acetonyl>amino>benzoate oxime

: 101760-54-7
ethyl p-acetonyl>amino>benzoate hydrochloride

Guidance literature:: With hydrogenchloride; In trifluoroacetic acid; at 65 - 70 ℃;
DOI:10.1021/jm00157a600

Reference yield:

: 101760-50-3
ethyl p-benzoate oxime

: 101760-54-7
ethyl p-acetonyl>amino>benzoate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 2.) N-methylmorpholine / methanol / Heating; 1.) 45 min, 2.) 3 h

2: 3.54 g / 1 N HCl / trifluoroacetic acid / 65 - 70 °C

With 4-methyl-morpholine; hydrogenchloride; In methanol; trifluoroacetic acid;
DOI:10.1021/jm00157a600

Reference yield:

: 101760-48-9,101760-57-0
ethyl p-benzoate oxime

: 101760-54-7
ethyl p-acetonyl>amino>benzoate hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine / methanol / 72 h / 50 °C

2: 2.) N-methylmorpholine / methanol / Heating; 1.) 45 min, 2.) 3 h

3: 3.54 g / 1 N HCl / trifluoroacetic acid / 65 - 70 °C

With 4-methyl-morpholine; hydrogenchloride; hydrazine; In methanol; trifluoroacetic acid;
DOI:10.1021/jm00157a600