Fmoc-(S)-2-amino-hept-6-ynoic acid

Base Information

• Chemical Name: Fmoc-(S)-2-amino-hept-6-ynoic acid
• CAS No.: 1097192-05-6
• Molecular Formula: C₂₂H₂₁NO₄
• Molecular Weight: 363.413
• Hs Code.: 9999999999
• Mol file: 1097192-05-6.mol

Synonyms:2S-{[(9H-fluorenyl-9-ylmethoxy)carbonyl]amino}-6-heptynoic acid

Chemical Property of Fmoc-(S)-2-amino-hept-6-ynoic acid

Chemical Property:

• Boiling Point: 599.0±50.0 °C(Predicted)
• PKA: 3.82±0.21(Predicted)
• Density: 1.242±0.06 g/cm3(Predicted)

Purity/Quality:

99%, ^*data from raw suppliers

(S)-2-(((9H-fluoren-9-yl)methoxy)carbonylamino)hept-6-ynoicacid 98% ^*data from reagent suppliers

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Technology Process of Fmoc-(S)-2-amino-hept-6-ynoic acid

There total 1 articles about Fmoc-(S)-2-amino-hept-6-ynoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide (82911-69-1) + (S)-bishomopropargylglycine (121703-79-5,211054-03-4,835627-45-7) → 2S-{[(9H-fluorenyl-9-ylmethoxy)carbonyl]amino}-6-heptynoic acid (1097192-05-6)

Guidance literature:

With sodium hydroxide; In 1,4-dioxane; water; at 20 ℃; for 4h; pH=8;

DOI:10.1002/ejoc.200800717

Reference yield:

2S-{[(9H-fluorenyl-9-ylmethoxy)carbonyl]amino}-6-heptynoic acid (1097192-05-6) + N-(fluoren-9-ylmethoxycarbonyl)glycine (29022-11-5) + Fmoc-Val-OH (68858-20-8) + (S)-2-[{({9H-fluoren-9-yl}methoxy)carbonyl}amino]pentanedioic acid (104091-09-0,136083-74-4,121343-82-6) + Fmoc-Trp-OH (35737-15-6) + Fmoc-Thr-OH (73731-37-0) + Fmoc-Asn-OH (71989-16-7) + Fmoc-Lys-OH (105047-45-8) + N-(9H-fluoren-9-ylmethoxycarbonyl)-L-serine (73724-45-5) + (S)-2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-azidopropanoic acid (684270-46-0) → C60H94N20O18

Guidance literature:

Fmoc-Lys-OH; With acetic anhydride; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In 1-methyl-pyrrolidin-2-one; for 0.333333h;

With piperidine; In N,N-dimethyl-formamide; for 0.0833333h;

2S-{[(9H-fluorenyl-9-ylmethoxy)carbonyl]amino}-6-heptynoic acid; N-(fluoren-9-ylmethoxycarbonyl)glycine; Fmoc-Val-OH; (S)-2-[{({9H-fluoren-9-yl}methoxy)carbonyl}amino]pentanedioic acid; Fmoc-Trp-OH; Fmoc-Thr-OH; Fmoc-Asn-OH; N-(9H-fluoren-9-ylmethoxycarbonyl)-L-serine; (S)-2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-3-azidopropanoic acid; Further stages;

DOI:10.1002/chem.201600154

Reference yield:

(S)-2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-4-azidobutanoic acid (942518-20-9) + 2S-{[(9H-fluorenyl-9-ylmethoxy)carbonyl]amino}-6-heptynoic acid (1097192-05-6) + N-(fluoren-9-ylmethoxycarbonyl)glycine (29022-11-5) + Fmoc-Val-OH (68858-20-8) + (S)-2-[{({9H-fluoren-9-yl}methoxy)carbonyl}amino]pentanedioic acid (104091-09-0,136083-74-4,121343-82-6) + Fmoc-Trp-OH (35737-15-6) + Fmoc-Thr-OH (73731-37-0) + Fmoc-Asn-OH (71989-16-7) + Fmoc-Lys-OH (105047-45-8) + N-(9H-fluoren-9-ylmethoxycarbonyl)-L-serine (73724-45-5) → C61H96N20O18

Guidance literature:

Fmoc-Lys-OH; With acetic anhydride; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In 1-methyl-pyrrolidin-2-one; for 0.333333h;

With piperidine; In N,N-dimethyl-formamide; for 0.0833333h;

(S)-2-((((9H-fluoren-9-yl)methoxy)carbonyl)amino)-4-azidobutanoic acid; 2S-{[(9H-fluorenyl-9-ylmethoxy)carbonyl]amino}-6-heptynoic acid; N-(fluoren-9-ylmethoxycarbonyl)glycine; Fmoc-Val-OH; (S)-2-[{({9H-fluoren-9-yl}methoxy)carbonyl}amino]pentanedioic acid; Fmoc-Trp-OH; Fmoc-Thr-OH; Fmoc-Asn-OH; N-(9H-fluoren-9-ylmethoxycarbonyl)-L-serine; Further stages;

DOI:10.1002/chem.201600154

upstream raw materials:

N-(9H-fluoren-2-ylmethoxycarbonyloxy)succinimide

(S)-bishomopropargylglycine

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