[Fe(CO)3(COOCH(C₅H₁₁)CHCHCHC(O)CH₂CH(OSi(CH₃)2C(CH₃)3)CH₂CH₂OCH₂C₆H₅)]

Base Information

Chemical Name:[Fe(CO)3(COOCH(C₅H₁₁)CHCHCHC(O)CH₂CH(OSi(CH₃)2C(CH₃)3)CH₂CH₂OCH₂C₆H₅)]
CAS No.:637030-97-8
Molecular Formula:C₃₁H₄₄FeO₈Si
Molecular Weight:628.618
Hs Code.:

[Fe(CO)3(COOCH(C<sub>5</sub>H<sub>11</sub>)CHCHCHC(O)CH<sub>2</sub>CH(OSi(CH<sub>3</sub>)2C(CH<sub>3</sub>)3)CH<sub>2</sub>CH<sub>2</sub>OCH<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)]

Synonyms:[Fe(CO)3(COOCH(C₅H₁₁)CHCHCHC(O)CH₂CH(OSi(CH₃)2C(CH₃)3)CH₂CH₂OCH₂C₆H₅)]

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Chemical Property of [Fe(CO)3(COOCH(C₅H₁₁)CHCHCHC(O)CH₂CH(OSi(CH₃)2C(CH₃)3)CH₂CH₂OCH₂C₆H₅)]

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Technology Process of [Fe(CO)3(COOCH(C₅H₁₁)CHCHCHC(O)CH₂CH(OSi(CH₃)2C(CH₃)3)CH₂CH₂OCH₂C₆H₅)]

There total 1 articles about [Fe(CO)3(COOCH(C₅H₁₁)CHCHCHC(O)CH₂CH(OSi(CH₃)2C(CH₃)3)CH₂CH₂OCH₂C₆H₅)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 637030-89-8
[Fe(CO)3(COOCH(C₅H₁₁)CHCHCHCOCH₂CH(OH)CH₂CH₂OCH₂C₆H₅)]

: 69739-34-0
t-butyldimethylsiyl triflate

: 637030-97-8
[Fe(CO)3(COOCH(C₅H₁₁)CHCHCHC(O)CH₂CH(OSi(CH₃)2C(CH₃)3)CH₂CH₂OCH₂C₆H₅)]

Guidance literature:: With triethylamine; In dichloromethane; treatment of dichloromethane soln. of Fe(CO)3(COOCH(C5H11)(CH)3COCH2CH(OH)CH2CH2OBn) with TBSOTf in the presence of NEt3 at 0°C for 18 h;
DOI:10.1039/b308793j

Reference yield: 83.0%

: 637030-97-8
[Fe(CO)3(COOCH(C₅H₁₁)CHCHCHC(O)CH₂CH(OSi(CH₃)2C(CH₃)3)CH₂CH₂OCH₂C₆H₅)]

: 637030-90-1
[Fe(CO)3(COOCH(C₅H₁₁)CHCHCHCH(OH)CH₂CH(OSi(CH₃)2C(CH₃)3)CH₂CH₂OCH₂C₆H₅)]

Guidance literature:: With (t-Bu)3Al; In dichloromethane; toluene; treatment of Fe(CO)3(COOCH(C5H11)(CH)3C(O)CH2C(OTBS)CH2CH2OBn) with (t-Bu)3Al in toluene-dichloromethane mixt. at 0°C for 30 min;
DOI:10.1039/b308793j