<(diethoxyphosphoryl)methyl(ethoxy)phosphoryl>methyl 2,3,4,5,6-pentafluorobenzenesulfonate

Base Information

Chemical Name:<(diethoxyphosphoryl)methyl(ethoxy)phosphoryl>methyl 2,3,4,5,6-pentafluorobenzenesulfonate
CAS No.:240432-44-4
Molecular Formula:C₁₄H₁₉F₅O₈P₂S
Molecular Weight:504.306
Hs Code.:

Synonyms:<(diethoxyphosphoryl)methyl(ethoxy)phosphoryl>methyl 2,3,4,5,6-pentafluorobenzenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of <(diethoxyphosphoryl)methyl(ethoxy)phosphoryl>methyl 2,3,4,5,6-pentafluorobenzenesulfonate

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Technology Process of <(diethoxyphosphoryl)methyl(ethoxy)phosphoryl>methyl 2,3,4,5,6-pentafluorobenzenesulfonate

There total 2 articles about <(diethoxyphosphoryl)methyl(ethoxy)phosphoryl>methyl 2,3,4,5,6-pentafluorobenzenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 832-53-1
pentafluorobenzenesulonyl chloride

: 240432-42-2
ethyl <(diethoxyphosphoryl)methyl>hydroxymethylphosphinate

: 240432-44-4
<(diethoxyphosphoryl)methyl(ethoxy)phosphoryl>methyl 2,3,4,5,6-pentafluorobenzenesulfonate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 - -15 ℃; for 15h;
DOI:10.1021/jm991008q

Reference yield:

: 240432-41-1
ethyl benzyloxymethyl<(diethoxyphosphoryl)methyl>phosphinate

: 240432-44-4
<(diethoxyphosphoryl)methyl(ethoxy)phosphoryl>methyl 2,3,4,5,6-pentafluorobenzenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 3.0 g / H₂ / 5 percent Pd/C/50 percent H₂O / ethanol / 12 h / 760 Torr

2: 84 percent / N-ethyldiisopropylamine / CH₂Cl₂ / 15 h / -78 - -15 °C

With hydrogen; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; water; In ethanol; dichloromethane;
DOI:10.1021/jm991008q