(E)-6-methyl-6-nitro-2-[[(phenylmethoxy)carbonyl]amino]-2-heptenoic acid methyl ester

Base Information

Chemical Name:(E)-6-methyl-6-nitro-2-[[(phenylmethoxy)carbonyl]amino]-2-heptenoic acid methyl ester
CAS No.:606147-37-9
Molecular Formula:C₁₇H₂₂N₂O₆
Molecular Weight:350.371
Hs Code.:

Synonyms:(E)-6-methyl-6-nitro-2-[[(phenylmethoxy)carbonyl]amino]-2-heptenoic acid methyl ester

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Chemical Property of (E)-6-methyl-6-nitro-2-[[(phenylmethoxy)carbonyl]amino]-2-heptenoic acid methyl ester

Chemical Property:

Purity/Quality:

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Technology Process of (E)-6-methyl-6-nitro-2-[[(phenylmethoxy)carbonyl]amino]-2-heptenoic acid methyl ester

There total 2 articles about (E)-6-methyl-6-nitro-2-[[(phenylmethoxy)carbonyl]amino]-2-heptenoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 57620-49-2
4-methyl-4-nitropentanal

: 100945-15-1,88568-95-0
N-(benzyloxycarbonyl)phosphonoglycine trimethyl ester

: 606147-37-9
(E)-6-methyl-6-nitro-2-[[(phenylmethoxy)carbonyl]amino]-2-heptenoic acid methyl ester

Guidance literature:: N-(benzyloxycarbonyl)phosphonoglycine trimethyl ester; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at -20 ℃; for 0.0833333h;

4-methyl-4-nitropentanal; In dichloromethane; at -20 - 20 ℃; for 21h;

Reference yield:

: 606147-23-3
2,6-dinitro-2,6-dimethyl-3-heptanol

: 100945-15-1,88568-95-0
N-(benzyloxycarbonyl)phosphonoglycine trimethyl ester

: 606147-37-9
(E)-6-methyl-6-nitro-2-[[(phenylmethoxy)carbonyl]amino]-2-heptenoic acid methyl ester

: 606147-24-4
(Z)-6-methyl-6-nitro-2-[[(phenylmethoxy)carbonyl]amino]-2-heptenoic acid methyl ester

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at -20 - 20 ℃;
DOI:10.1021/ol0352308

Reference yield:

: 606147-37-9
(E)-6-methyl-6-nitro-2-[[(phenylmethoxy)carbonyl]amino]-2-heptenoic acid methyl ester

: 606147-25-5
(S)-6-methyl-6-nitro-2-[[(phenylmethoxy)carbonyl]amino]heptanoic acid methyl ester

Guidance literature:: With hydrogen; 1,2-bis((2S,5S)-2,5-dimethylphospholano)benzene(cyclooctadiene)rhodium(I) tetrafluoroborate; In methanol; at 20 ℃; for 24h; under 2585.81 Torr;