N¹-((benzylcarbamoyl)oxy)-3-(2,4-dichlorophenyl)-N⁵-(o-tolyl)pentanediamide

Base Information

Chemical Name:N¹-((benzylcarbamoyl)oxy)-3-(2,4-dichlorophenyl)-N⁵-(o-tolyl)pentanediamide
CAS No.:1551577-87-7
Molecular Formula:C₂₆H₂₅Cl₂N₃O₄
Molecular Weight:514.408
Hs Code.:

N<SUP>1</SUP>-((benzylcarbamoyl)oxy)-3-(2,4-dichlorophenyl)-N<SUP>5</SUP>-(o-tolyl)pentanediamide

Synonyms:N¹-((benzylcarbamoyl)oxy)-3-(2,4-dichlorophenyl)-N⁵-(o-tolyl)pentanediamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N¹-((benzylcarbamoyl)oxy)-3-(2,4-dichlorophenyl)-N⁵-(o-tolyl)pentanediamide

Chemical Property:

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Technology Process of N¹-((benzylcarbamoyl)oxy)-3-(2,4-dichlorophenyl)-N⁵-(o-tolyl)pentanediamide

There total 10 articles about N¹-((benzylcarbamoyl)oxy)-3-(2,4-dichlorophenyl)-N⁵-(o-tolyl)pentanediamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₉H₁₆Cl₂N₂O₄

: 100-46-9
benzylamine

: 1551577-87-7
N¹-((benzylcarbamoyl)oxy)-3-(2,4-dichlorophenyl)-N⁵-(o-tolyl)pentanediamide

Guidance literature:: In acetonitrile; at 20 ℃;
DOI:10.1016/j.bmc.2013.11.053

Reference yield:

: C₁₃H₉Cl₂F₃O₅

: 1551577-87-7
N¹-((benzylcarbamoyl)oxy)-3-(2,4-dichlorophenyl)-N⁵-(o-tolyl)pentanediamide

Guidance literature:: Multi-step reaction with 6 steps

1: triethylamine / 0 - 20 °C

2: N,N-dimethyl-formamide; oxalyl dichloride / chloroform / 1 h / 0 - 20 °C

3: triethylamine; dmap / chloroform / 0 - 20 °C

4: potassium cyanide; hydroxylamine / tetrahydrofuran; water; methanol / 20 °C

5: acetonitrile / 0.5 h / 0 °C

6: acetonitrile / 20 °C

With dmap; potassium cyanide; oxalyl dichloride; hydroxylamine; triethylamine; N,N-dimethyl-formamide; In tetrahydrofuran; methanol; chloroform; water; acetonitrile;
DOI:10.1016/j.bmc.2013.11.053

Reference yield:

: 1551577-60-6
methyl 3-(2,4-dichlorophenyl)-5-oxo-5-(o-tolylamino)pentanoate

: 1551577-87-7
N¹-((benzylcarbamoyl)oxy)-3-(2,4-dichlorophenyl)-N⁵-(o-tolyl)pentanediamide

Guidance literature:: Multi-step reaction with 3 steps

1: potassium cyanide; hydroxylamine / tetrahydrofuran; water; methanol / 20 °C

2: acetonitrile / 0.5 h / 0 °C

3: acetonitrile / 20 °C

With potassium cyanide; hydroxylamine; In tetrahydrofuran; methanol; water; acetonitrile;
DOI:10.1016/j.bmc.2013.11.053