O-benzyl-N-Boc-N,2,6-trimethyl-tyrosyl-N-(3-phenylpropyl)-D-alaninamide

Base Information

Chemical Name:O-benzyl-N-Boc-N,2,6-trimethyl-tyrosyl-N-(3-phenylpropyl)-D-alaninamide
CAS No.:111633-08-0
Molecular Formula:C₃₆H₄₇N₃O₅
Molecular Weight:601.786
Hs Code.:

Synonyms:O-benzyl-N-Boc-N,2,6-trimethyl-tyrosyl-N-(3-phenylpropyl)-D-alaninamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O-benzyl-N-Boc-N,2,6-trimethyl-tyrosyl-N-(3-phenylpropyl)-D-alaninamide

Chemical Property:

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Technology Process of O-benzyl-N-Boc-N,2,6-trimethyl-tyrosyl-N-(3-phenylpropyl)-D-alaninamide

There total 5 articles about O-benzyl-N-Boc-N,2,6-trimethyl-tyrosyl-N-(3-phenylpropyl)-D-alaninamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 194857-87-9
O-benzyl-N-Boc-N,2,6-trimethyltyrosine

: 111633-08-0
O-benzyl-N-Boc-N,2,6-trimethyl-tyrosyl-N-(3-phenylpropyl)-D-alaninamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 5A molecular sieves, N-methylmorpholine / 1.) CH₂Cl₂, a) -15 deg C - 5 deg C, b) 5 deg C - -60 deg C, 2.) CH₂Cl₂, 0 deg C, 30 min

2: NMM / CH₂Cl₂ / 1.) -55 deg - RT, 2.) RT, 1.5 h

With 4-methyl-morpholine; 5A molecular sieve; In dichloromethane;

Reference yield:

: 111648-92-1
3-(4-Benzyloxy-2,6-dimethyl-phenyl)-2-tert-butoxycarbonylamino-propionic acid benzyl ester

: 111633-08-0
O-benzyl-N-Boc-N,2,6-trimethyl-tyrosyl-N-(3-phenylpropyl)-D-alaninamide

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) sodium hydride / 1.) DMF, 15 min, 2.) DMF, 2.5 h

2: 0.70 g / aq. NaOH / methanol

3: 1.) 5A molecular sieves, N-methylmorpholine / 1.) CH₂Cl₂, a) -15 deg C - 5 deg C, b) 5 deg C - -60 deg C, 2.) CH₂Cl₂, 0 deg C, 30 min

4: NMM / CH₂Cl₂ / 1.) -55 deg - RT, 2.) RT, 1.5 h

With 4-methyl-morpholine; sodium hydroxide; 5A molecular sieve; sodium hydride; In methanol; dichloromethane;

Reference yield:

: 155921-00-9
O-benzyl-N-Boc-N,2,6-trimethyl-DL-tyrosine benzyl eter

: 111633-08-0
O-benzyl-N-Boc-N,2,6-trimethyl-tyrosyl-N-(3-phenylpropyl)-D-alaninamide

Guidance literature:: Multi-step reaction with 3 steps

1: 0.70 g / aq. NaOH / methanol

2: 1.) 5A molecular sieves, N-methylmorpholine / 1.) CH₂Cl₂, a) -15 deg C - 5 deg C, b) 5 deg C - -60 deg C, 2.) CH₂Cl₂, 0 deg C, 30 min

3: NMM / CH₂Cl₂ / 1.) -55 deg - RT, 2.) RT, 1.5 h

With 4-methyl-morpholine; sodium hydroxide; 5A molecular sieve; In methanol; dichloromethane;