1,2,3,4-tetrahydro-3,3-dimethylpyrido<3,4-e>-1,2,4-triazine dihydrochloride

Base Information

Chemical Name:1,2,3,4-tetrahydro-3,3-dimethylpyrido<3,4-e>-1,2,4-triazine dihydrochloride
CAS No.:121845-85-0
Molecular Formula:C₈H₁₂N₄*2ClH
Molecular Weight:237.132
Hs Code.:

Synonyms:1,2,3,4-tetrahydro-3,3-dimethylpyrido<3,4-e>-1,2,4-triazine dihydrochloride

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Chemical Property of 1,2,3,4-tetrahydro-3,3-dimethylpyrido<3,4-e>-1,2,4-triazine dihydrochloride

Chemical Property:

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MSDS Files:: SDS file from LookChem

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Technology Process of 1,2,3,4-tetrahydro-3,3-dimethylpyrido<3,4-e>-1,2,4-triazine dihydrochloride

There total 1 articles about 1,2,3,4-tetrahydro-3,3-dimethylpyrido<3,4-e>-1,2,4-triazine dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5435-54-1
4-hydroxy-3-nitropyridine

: 121845-85-0
1,2,3,4-tetrahydro-3,3-dimethylpyrido<3,4-e>-1,2,4-triazine dihydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / PCl₅, POCl₃ / 6 h / 130 - 140 °C

2: 77 percent / N₂H₄*H₂O / ethanol / 1.) 0 deg C, 0.75 h, 2.) 25 deg C, 3.5 h

3: 4.9 g / H₂ / 5percent Pd/C / aq. ethanol

4: 69 percent / HCl / ethanol / 1.) overnight, 2.) reflux, 1 h

With hydrogenchloride; phosphorus pentachloride; hydrogen; hydrazine hydrate; trichlorophosphate; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00131a010