1,3-dihydro-3-methyl-1-p-tolyl-(1,2,3-tri-O-acetyl-4-S-acetyl-4-thio-D-arabino-tetritol-1-yl)-2H-imidazole-2-thione

Base Information

Chemical Name:1,3-dihydro-3-methyl-1-p-tolyl-(1,2,3-tri-O-acetyl-4-S-acetyl-4-thio-D-arabino-tetritol-1-yl)-2H-imidazole-2-thione
CAS No.:116384-45-3
Molecular Formula:C₂₃H₂₈N₂O₇S₂
Molecular Weight:508.617
Hs Code.:

Synonyms:1,3-dihydro-3-methyl-1-p-tolyl-(1,2,3-tri-O-acetyl-4-S-acetyl-4-thio-D-arabino-tetritol-1-yl)-2H-imidazole-2-thione

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Chemical Property of 1,3-dihydro-3-methyl-1-p-tolyl-(1,2,3-tri-O-acetyl-4-S-acetyl-4-thio-D-arabino-tetritol-1-yl)-2H-imidazole-2-thione

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Technology Process of 1,3-dihydro-3-methyl-1-p-tolyl-(1,2,3-tri-O-acetyl-4-S-acetyl-4-thio-D-arabino-tetritol-1-yl)-2H-imidazole-2-thione

There total 1 articles about 1,3-dihydro-3-methyl-1-p-tolyl-(1,2,3-tri-O-acetyl-4-S-acetyl-4-thio-D-arabino-tetritol-1-yl)-2H-imidazole-2-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 116384-44-2
Acetic acid (1R,2S,3R)-2,3-diacetoxy-1-(3-methyl-2-thioxo-1-p-tolyl-2,3-dihydro-1H-imidazol-4-yl)-4-(toluene-4-sulfonyloxy)-butyl ester

: 10387-40-3
potassium thioacetate

: 116384-45-3
1,3-dihydro-3-methyl-1-p-tolyl-(1,2,3-tri-O-acetyl-4-S-acetyl-4-thio-D-arabino-tetritol-1-yl)-2H-imidazole-2-thione

Guidance literature:: In butanone; for 4h; Yield given; Heating;
DOI:10.1016/S0008-6215(00)90799-7

Reference yield: 97.0%

: 116384-45-3
1,3-dihydro-3-methyl-1-p-tolyl-(1,2,3-tri-O-acetyl-4-S-acetyl-4-thio-D-arabino-tetritol-1-yl)-2H-imidazole-2-thione

: 116384-47-5
4,4'-dithiobis<4-(4-deoxy-D-arabino-tetritol-1-yl)-1,3-dihydro-3-methyl-1-p-tolyl-2H-imidazole-2-thione>

Guidance literature:: With sodium methylate; In methanol; for 24h; Ambient temperature;
DOI:10.1016/S0008-6215(00)90799-7

Reference yield:

: 116384-45-3
1,3-dihydro-3-methyl-1-p-tolyl-(1,2,3-tri-O-acetyl-4-S-acetyl-4-thio-D-arabino-tetritol-1-yl)-2H-imidazole-2-thione

: 116384-50-0
1,3-dihydro-3-methyl-4-(4-thio-2,3-di-O-p-tolylsulphonyl-α-D-erythrofuranosyl)-1-p-tolyl-2H-imidazole-2-thione

Guidance literature:: Multi-step reaction with 3 steps

1: sodium methoxide / methanol / 0.08 h / Ambient temperature

2: trifluoroacetic acid / aq. ethanol / 3 h / Heating

3: 24 percent / pyridine / 24 h / 0 °C

With sodium methylate; trifluoroacetic acid; In pyridine; methanol; ethanol;
DOI:10.1016/S0008-6215(00)90799-7