Ru(HOC₂H₅)N₄C₂₀H₈(C₆H₅)4(CS)

Base Information

Chemical Name:Ru(HOC₂H₅)N₄C₂₀H₈(C₆H₅)4(CS)
CAS No.:148603-21-8
Molecular Formula:C₄₇H₃₄N₄ORuS
Molecular Weight:803.949
Hs Code.:

Ru(HOC<sub>2</sub>H<sub>5</sub>)N<sub>4</sub>C<sub>20</sub>H<sub>8</sub>(C<sub>6</sub>H<sub>5</sub>)4(CS)

Synonyms:Ru(HOC₂H₅)N₄C₂₀H₈(C₆H₅)4(CS)

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Chemical Property of Ru(HOC₂H₅)N₄C₂₀H₈(C₆H₅)4(CS)

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Technology Process of Ru(HOC₂H₅)N₄C₂₀H₈(C₆H₅)4(CS)

There total 3 articles about Ru(HOC₂H₅)N₄C₂₀H₈(C₆H₅)4(CS) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 463-71-8
thiophosgene

: [Ru(meso-5,10,15,20-tetraphenylporphyrinate)(OEt)]2(μ-O) * 2 H2O

: 148603-21-8
Ru(HOC₂H₅)N₄C₂₀H₈(C₆H₅)4(CS)

Guidance literature:: With amalgamated zinc; In dichloromethane; addn. of zinc amalgam powder to complex in CH2Cl2 at 298 K, stirred for 30 min, addn. of CSCl2 in CH2Cl2, stirred for 4 h; monitored by UV and IR, filtered, addn. of EtOH, rotary evapd. to dryness, column chromy. (alumina/CH2Cl2, CCl4), evapd. to dryness, recrystd. from CH2Cl2/EtOH/n-C6H14;
DOI:10.1016/S0277-5387(00)81764-7

Reference yield: 60.0%

: [Ru(meso-5,10,15,20-tetraphenylporphyrinate)(OEt)]2(μ-O) * 2 H2O

: 2976-37-6
benzyl trichloromethyl thioether

: 148603-21-8
Ru(HOC₂H₅)N₄C₂₀H₈(C₆H₅)4(CS)

Guidance literature:: iron(II) chloride; In ethanol; toluene; complex in toluene reduced for 30 min under N2, addn. of thioether in toluene, addn. of FeCl2 in EtOH, react. for 48 h; react. monitored by absorption spectroscopy, filtered through Celite, rotary evapd., column chromy. (alumina/CH2Cl2-CCl4), evapd. to dryness, crystd. from CH2Cl2/EtOH/n-hexane; elem. anal.;
DOI:10.1016/S0277-5387(00)81764-7

Reference yield: 30.0%

: [Ru(meso-5,10,15,20-tetraphenylporphyrinate)(OEt)]2(μ-O) * 2 H2O

: 148603-21-8
Ru(HOC₂H₅)N₄C₂₀H₈(C₆H₅)4(CS)

Guidance literature:: With carbon disulfide; sodium amalgam; In tetrahydrofuran; addn. of Na/Hg to complex in THF (15 min purged with N2), stirred for 30 min, addn. of CS2, stirred under N2 for 48 h; filtered through Celite, rotary evapd., repeatedly column chromy. (alumina/toluene);
DOI:10.1016/S0277-5387(00)81764-7