C₂₅H₂₇NO₆S

Base Information

Chemical Name:C₂₅H₂₇NO₆S
CAS No.:1275597-30-2
Molecular Formula:C₂₅H₂₇NO₆S
Molecular Weight:469.558
Hs Code.:

C<sub>25</sub>H<sub>27</sub>NO<sub>6</sub>S

Synonyms:C₂₅H₂₇NO₆S

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Chemical Property of C₂₅H₂₇NO₆S

Chemical Property:

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Technology Process of C₂₅H₂₇NO₆S

There total 8 articles about C₂₅H₂₇NO₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1275597-29-9
C₂₅H₂₇NO₅S

: 1275597-30-2
C₂₅H₂₇NO₆S

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at -78 ℃; for 0.25h;
DOI:10.1021/jo1022487

Reference yield:

: 16617-07-5
naltrexone methyl ether

: 1275597-30-2
C₂₅H₂₇NO₆S

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium tris(acetoxy)borohydride; acetic acid / 0.5 h / 0 °C / Inert atmosphere

2.1: pyridine / 0.25 h / 0 °C / Inert atmosphere

3.1: potassium tert-butylate / tetrahydrofuran / 12 h / 0 - 20 °C / Inert atmosphere

4.1: lithium triethylborohydride / tetrahydrofuran / 24 h / 0 - 60 °C / Inert atmosphere

4.2: 1 h / 0 °C / Reflux

5.1: 1 h / Inert atmosphere; Reflux

6.1: potassium carbonate / 1,1,2,2-tetrachloroethane / 12 h / 150 °C / Inert atmosphere

7.1: potassium hydroxide / water; dimethyl sulfoxide / 12 h / 110 °C / Inert atmosphere

8.1: N-chloro-succinimide / chloroform / 0.5 h / -30 °C / Inert atmosphere

9.1: 15-crown-5; sodium hydride / tetrahydrofuran / 20 °C / Inert atmosphere

9.2: 11 h

10.1: lithium diisopropyl amide / tetrahydrofuran; hexane] / 1 h / -78 - 0 °C / Inert atmosphere

10.2: 2.5 h / 20 °C / Inert atmosphere

11.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.25 h / -78 °C

With pyridine; N-chloro-succinimide; 15-crown-5; potassium tert-butylate; sodium tris(acetoxy)borohydride; sodium hydride; lithium triethylborohydride; potassium carbonate; acetic acid; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; chloroform; hexane]; water; dimethyl sulfoxide; 1,1,2,2-tetrachloroethane; 9.1: Grob fragmentation;
DOI:10.1021/jo1022487

Reference yield:

: C₂₁H₂₆INO₃

: 1275597-30-2
C₂₅H₂₇NO₆S

Guidance literature:: Multi-step reaction with 8 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 16 h / 100 °C / Inert atmosphere

1.2: 30 h / 20 °C

2.1: 1 h / Inert atmosphere; Reflux

3.1: potassium carbonate / 1,1,2,2-tetrachloroethane / 12 h / 150 °C / Inert atmosphere

4.1: potassium hydroxide / water; dimethyl sulfoxide / 12 h / 110 °C / Inert atmosphere

5.1: N-chloro-succinimide / chloroform / 0.5 h / -30 °C / Inert atmosphere

6.1: 15-crown-5; sodium hydride / tetrahydrofuran / 20 °C / Inert atmosphere

6.2: 11 h

7.1: lithium diisopropyl amide / tetrahydrofuran; hexane] / 1 h / -78 - 0 °C / Inert atmosphere

7.2: 2.5 h / 20 °C / Inert atmosphere

8.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.25 h / -78 °C

With N-chloro-succinimide; 15-crown-5; sodium hydride; potassium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; 3-chloro-benzenecarboperoxoic acid; potassium hydroxide; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane; chloroform; hexane]; water; dimethyl sulfoxide; N,N-dimethyl-formamide; 1,1,2,2-tetrachloroethane; 6.1: Grob fragmentation;
DOI:10.1021/jo1022487