15-benzyloxy-7-methyl-3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene

Base Information

• Chemical Name: 15-benzyloxy-7-methyl-3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene
• CAS No.: 1257225-63-0
• Molecular Formula: C₂₁H₃₀N₄O
• Molecular Weight: 354.495

Synonyms:15-benzyloxy-7-methyl-3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene

Chemical Property of 15-benzyloxy-7-methyl-3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene

Chemical Property:

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Technology Process of 15-benzyloxy-7-methyl-3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene

There total 1 articles about 15-benzyloxy-7-methyl-3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1⁽¹⁷⁾,13,15-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

3,3'-Diamino-N-methyldipropylamine (105-83-9) + 4-(benzyloxy)pyridine-2,6-dicarboxaldehyde (130567-64-5) → 15-benzyloxy-7-methyl-3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1(17),13,15-triene (1257225-63-0)

Guidance literature:

3,3'-Diamino-N-methyldipropylamine; 4-(benzyloxy)pyridine-2,6-dicarboxaldehyde; With copper(II) nitrate trihydrate; In ethanol; water; at 60 ℃; for 6h;

With sodium tetrahydroborate; In methanol; water; Further stages;

DOI:10.1016/j.ica.2010.05.051

Reference yield: 28.0%

nickel(II) perchlorate hexahydrate + 15-benzyloxy-7-methyl-3,7,11,17-tetraaza-bicyclo[11.3.1]heptadeca-1(17),13,15-triene (1257225-63-0) → Ni(15-benzyloxy-7-methyl-3,7,11,17-tetraazabicyclo[11.3.1]heptadeca-1(17),13,15-triene)(ClO4)2

Guidance literature:

In methanol; to MeOH soln. of tetraaza-compd. added MeOH soln. of Ni(ClO4)2*6H2O; mixt. heated at 60°C for 30 min; then cooled in ice bath; recrystd. from MeNO2/EtOAc; elem. anal.;

DOI:10.1016/j.ica.2010.05.051

upstream raw materials:

3,3'-Diamino-N-methyldipropylamine

4-(benzyloxy)pyridine-2,6-dicarboxaldehyde

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