2,3-di-O-benzyl-4,6-O-benzylidene-1-deoxy-1-(2-oxo-2-phenylethyl)-β-D-mannopyranose

Base Information

Chemical Name:2,3-di-O-benzyl-4,6-O-benzylidene-1-deoxy-1-(2-oxo-2-phenylethyl)-β-D-mannopyranose
CAS No.:1072522-97-4
Molecular Formula:C₃₅H₃₄O₆
Molecular Weight:550.651
Hs Code.:

Synonyms:2,3-di-O-benzyl-4,6-O-benzylidene-1-deoxy-1-(2-oxo-2-phenylethyl)-β-D-mannopyranose

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Chemical Property of 2,3-di-O-benzyl-4,6-O-benzylidene-1-deoxy-1-(2-oxo-2-phenylethyl)-β-D-mannopyranose

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Technology Process of 2,3-di-O-benzyl-4,6-O-benzylidene-1-deoxy-1-(2-oxo-2-phenylethyl)-β-D-mannopyranose

There total 3 articles about 2,3-di-O-benzyl-4,6-O-benzylidene-1-deoxy-1-(2-oxo-2-phenylethyl)-β-D-mannopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 13735-81-4
1-styrenyloxytrimethylsilane

: 159407-17-7
phenyl 2,3-di-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

: 1072522-97-4
2,3-di-O-benzyl-4,6-O-benzylidene-1-deoxy-1-(2-oxo-2-phenylethyl)-β-D-mannopyranose

Guidance literature:: phenyl 2,3-di-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside; With trifluoromethylsulfonic anhydride; 1,1'-sulfinylbisbenzene; 2,4,6-tri-tert-butylpyrimidine; In dichloromethane; at -65 ℃; for 0.75h; Molecular sieve;

1-styrenyloxytrimethylsilane; In dichloromethane; at -65 ℃; Molecular sieve;
DOI:10.1021/jo3011655

Reference yield:

: 13735-81-4
1-styrenyloxytrimethylsilane

: 314740-77-7
2,3-di-O-benzyl-4,6-O-benzylidene-α-D-mannopyranosyl triflate

: 1072522-97-4
2,3-di-O-benzyl-4,6-O-benzylidene-1-deoxy-1-(2-oxo-2-phenylethyl)-β-D-mannopyranose

Guidance literature:: In dichloromethane; at -60 ℃; for 2h; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol8017038

Reference yield:

: 2,3-di-O-benzyl-4,6-O-benzylidene-D-mannopyranosyl picolinate

: 1-Phenyl-3-trimethylsilanyloxy-but-3-en-1-one

: 1072522-97-4
2,3-di-O-benzyl-4,6-O-benzylidene-1-deoxy-1-(2-oxo-2-phenylethyl)-β-D-mannopyranose

: 2,3-di-O-benzyl-4,6-O-benzylidene-1-deoxy-1-(2-oxo-2-phenylethyl)-D-mannopyranose

Guidance literature:: With copper(II) bis(trifluoromethanesulfonate); In dichloromethane; at 20 ℃; Overall yield = 51percent; Overall yield = 28 mg; stereoselective reaction; Molecular sieve; Inert atmosphere; Sealed tube;
DOI:10.1021/acs.joc.0c01041