C₅₀H₇₁N₅O₁₃

Base Information

Chemical Name:C₅₀H₇₁N₅O₁₃
CAS No.:118878-64-1
Molecular Formula:C₅₀H₇₁N₅O₁₃
Molecular Weight:950.139
Hs Code.:

C<sub>50</sub>H<sub>71</sub>N<sub>5</sub>O<sub>13</sub>

Synonyms:C₅₀H₇₁N₅O₁₃

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Chemical Property of C₅₀H₇₁N₅O₁₃

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Technology Process of C₅₀H₇₁N₅O₁₃

There total 29 articles about C₅₀H₇₁N₅O₁₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 118919-23-6
C₅₀H₇₁N₅O₁₃

: 118878-64-1
C₅₀H₇₁N₅O₁₃

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃;
DOI:10.1055/s-1991-26448

Reference yield:

: 118878-59-4,118919-20-3
H-(2RS,4S)-Hip-Leu-OTCE

: 118878-64-1
C₅₀H₇₁N₅O₁₃

Guidance literature:: Multi-step reaction with 9 steps

1: 95 percent / dicyclohexylcarbodiimide / 4-dimethylaminopyridine / CH₂Cl₂ / 20 h / -20 deg C -> 20 deg C

2: 50 percent aq. HF / acetonitrile / 15 h / 20 °C

3: 6 N HCl / dioxane / 1 h / 20 °C

4: 70 percent / N,N-bis<2-oxo-3-oxazolidinyl>phosphorodiamidic chloride, N-ethyldiisopropylamine / CH₂Cl₂ / 15 h / 0 deg C -> room temperature

5: 100 percent / Zn-powder, 90 percent aq. AcOH / 15 h / 20 °C

6: dicyclohexylcarbodiimide / CH₂Cl₂ / 15 h / -20 deg C -> 20 deg C

7: CH₂Cl₂ / 1 h / 0 °C

8: 1 N aq. NaHCO₃ / CH₂Cl₂; CHCl₃ / 0.08 h / 20 °C

9: 100 percent / CF₃COOH / CH₂Cl₂ / 20 °C

With hydrogenchloride; N,N-bis[2-oxo-3-oxazolidinyl]phosphorodiamidic chloride; hydrogen fluoride; sodium hydrogencarbonate; acetic acid; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; zinc; dmap; In 1,4-dioxane; dichloromethane; chloroform; acetonitrile;
DOI:10.1055/s-1991-26448

Reference yield:

: 110720-45-1
N-Boc-O-tert-butyldimethylsilyl-(3S,4R,5S)-isostatine

: 118878-64-1
C₅₀H₇₁N₅O₁₃

Guidance literature:: Multi-step reaction with 9 steps

1: 95 percent / dicyclohexylcarbodiimide / 4-dimethylaminopyridine / CH₂Cl₂ / 20 h / -20 deg C -> 20 deg C

2: 50 percent aq. HF / acetonitrile / 15 h / 20 °C

3: 6 N HCl / dioxane / 1 h / 20 °C

4: 70 percent / N,N-bis<2-oxo-3-oxazolidinyl>phosphorodiamidic chloride, N-ethyldiisopropylamine / CH₂Cl₂ / 15 h / 0 deg C -> room temperature

5: 100 percent / Zn-powder, 90 percent aq. AcOH / 15 h / 20 °C

6: dicyclohexylcarbodiimide / CH₂Cl₂ / 15 h / -20 deg C -> 20 deg C

7: CH₂Cl₂ / 1 h / 0 °C

8: 1 N aq. NaHCO₃ / CH₂Cl₂; CHCl₃ / 0.08 h / 20 °C

9: 100 percent / CF₃COOH / CH₂Cl₂ / 20 °C

With hydrogenchloride; N,N-bis[2-oxo-3-oxazolidinyl]phosphorodiamidic chloride; hydrogen fluoride; sodium hydrogencarbonate; acetic acid; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; trifluoroacetic acid; zinc; dmap; In 1,4-dioxane; dichloromethane; chloroform; acetonitrile;
DOI:10.1055/s-1991-26448