2-[(4-fluorophenyl)sulfonyl]ethoxy carbonyl chloride

Base Information

• Chemical Name: 2-[(4-fluorophenyl)sulfonyl]ethoxy carbonyl chloride
• CAS No.: 1239605-26-5
• Molecular Formula: C₉H₈ClFO₄S
• Molecular Weight: 266.678

Synonyms:2-[(4-fluorophenyl)sulfonyl]ethoxy carbonyl chloride

Chemical Property of 2-[(4-fluorophenyl)sulfonyl]ethoxy carbonyl chloride

Chemical Property:

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Technology Process of 2-[(4-fluorophenyl)sulfonyl]ethoxy carbonyl chloride

There total 1 articles about 2-[(4-fluorophenyl)sulfonyl]ethoxy carbonyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

bis(trichloromethyl) carbonate (32315-10-9) + 2-[(4-fluorophenyl)sulfonyl]ethanol (28122-13-6) → 2-[(4-fluorophenyl)sulfonyl]ethoxy carbonyl chloride (1239605-26-5)

Guidance literature:

With N,N-dimethyl-formamide; In acetonitrile; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.3390/molecules15085708

Reference yield: 85.0%

4-fluorobenzylic alcohol (459-56-3) + 2-[(4-fluorophenyl)sulfonyl]ethoxy carbonyl chloride (1239605-26-5) → 4-fluorobenzyl 2-[(4-fluorobenzyl)sulfonyl]ethylcarbonate (1239605-27-6)

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃; Inert atmosphere;

DOI:10.3390/molecules15085708

Reference yield: 68.0%

2-[(4-fluorophenyl)sulfonyl]ethoxy carbonyl chloride (1239605-26-5) + 4-methylphenyl 2,3-di-O-(4-fluorobenzoyl)-6-O-benzyl-1-thio-β-D-galactopyranoside → 4-methylphenyl 6-O-benzyl-2,3-di-O-(4-fluorobenzoyl)-4-O-[2-(4-fluorophenyl)sulfonylethoxycarbonyl]-1-thio-β-D-galactopyranoside (1239605-29-8)

Guidance literature:

With pyridine; In tetrahydrofuran; at 45 - 58 ℃; for 7h; Inert atmosphere;

DOI:10.3390/molecules15085708

upstream raw materials:

bis(trichloromethyl) carbonate

2-[(4-fluorophenyl)sulfonyl]ethanol

Downstream raw materials:

4-methylphenyl 6-O-benzyl-2,3-di-O-(4-fluorobenzoyl)-4-O-[2-(4-fluorophenyl)sulfonylethoxycarbonyl]-1-thio-β-D-galactopyranoside

4-fluorobenzyl 2-[(4-fluorobenzyl)sulfonyl]ethylcarbonate

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