3-(N-(1,2-dihydro-2-oxo-1-phenylquinoxalin-3-yl)-N-methylamino)-1-phenylquinoxalin-2(1H)-one

Base Information

• Chemical Name: 3-(N-(1,2-dihydro-2-oxo-1-phenylquinoxalin-3-yl)-N-methylamino)-1-phenylquinoxalin-2(1H)-one
• CAS No.: 1145685-41-1
• Molecular Formula: C₂₉H₂₁N₅O₂
• Molecular Weight: 471.518

Synonyms:3-(N-(1,2-dihydro-2-oxo-1-phenylquinoxalin-3-yl)-N-methylamino)-1-phenylquinoxalin-2(1H)-one

Chemical Property of 3-(N-(1,2-dihydro-2-oxo-1-phenylquinoxalin-3-yl)-N-methylamino)-1-phenylquinoxalin-2(1H)-one

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Technology Process of 3-(N-(1,2-dihydro-2-oxo-1-phenylquinoxalin-3-yl)-N-methylamino)-1-phenylquinoxalin-2(1H)-one

There total 1 articles about 3-(N-(1,2-dihydro-2-oxo-1-phenylquinoxalin-3-yl)-N-methylamino)-1-phenylquinoxalin-2(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

3-chloro-1-phenylquinoxalin-2(1H)-one (181863-42-3) + 3-(methylamino)-1-phenylquinoxalin-2(1H)-one (1145685-40-0) → 3-(N-(1,2-dihydro-2-oxo-1-phenylquinoxalin-3-yl)-N-methylamino)-1-phenylquinoxalin-2(1H)-one (1145685-41-1)

Guidance literature:

3-(methylamino)-1-phenylquinoxalin-2(1H)-one; With potassium hydride; In tetrahydrofuran; mineral oil; at -78 - 20 ℃; Inert atmosphere;

3-chloro-1-phenylquinoxalin-2(1H)-one; In tetrahydrofuran; mineral oil; Inert atmosphere; Reflux;

DOI:10.1002/chem.200901961

Reference yield: 26.0%

3-(N-(1,2-dihydro-2-oxo-1-phenylquinoxalin-3-yl)-N-methylamino)-1-phenylquinoxalin-2(1H)-one (1145685-41-1) → 5,7-bis-(phenyl)-13-methyl-5,13-dihydro-[5,6,7,12,13,14]-hexaazapentacenium chloride (1145685-42-2)

Guidance literature:

3-(N-(1,2-dihydro-2-oxo-1-phenylquinoxalin-3-yl)-N-methylamino)-1-phenylquinoxalin-2(1H)-one; With phosphorus pentachloride; In dichloromethane; at 20 ℃; for 12h;

With ammonia; In tetrahydrofuran; at 20 ℃; for 0.166667h;

With ammonium chloride; In N,N-dimethyl-formamide; at 160 ℃;

DOI:10.1002/chem.200901961

Reference yield:

trifluoromethylsulfonic anhydride (358-23-6) + 3-(N-(1,2-dihydro-2-oxo-1-phenylquinoxalin-3-yl)-N-methylamino)-1-phenylquinoxalin-2(1H)-one (1145685-41-1) → 2CF3O3S(1-)*C31H21F6N5O6S2(2+)

Guidance literature:

In dichloromethane; at 20 ℃; for 12h;

DOI:10.1002/chem.200901961

upstream raw materials:

3-chloro-1-phenylquinoxalin-2(1H)-one

3-(methylamino)-1-phenylquinoxalin-2(1H)-one

Downstream raw materials:

5,7-bis-(phenyl)-13-methyl-5,13-dihydro-[5,6,7,12,13,14]-hexaazapentacenium chloride

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