(5RS,6RS)-1-Methyl-3-oxa-5-tosyloxy-6-<1'-<(methoxy)methoxy>cinnamyl>-6-methoxy-2-piperidinone

Base Information

Chemical Name:(5RS,6RS)-1-Methyl-3-oxa-5-tosyloxy-6-<1'-<(methoxy)methoxy>cinnamyl>-6-methoxy-2-piperidinone
CAS No.:73089-58-4
Molecular Formula:C₂₄H₂₉NO₈S
Molecular Weight:491.562
Hs Code.:

Synonyms:(5RS,6RS)-1-Methyl-3-oxa-5-tosyloxy-6-<1'-<(methoxy)methoxy>cinnamyl>-6-methoxy-2-piperidinone

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Chemical Property of (5RS,6RS)-1-Methyl-3-oxa-5-tosyloxy-6-<1'-<(methoxy)methoxy>cinnamyl>-6-methoxy-2-piperidinone

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Technology Process of (5RS,6RS)-1-Methyl-3-oxa-5-tosyloxy-6-<1'-<(methoxy)methoxy>cinnamyl>-6-methoxy-2-piperidinone

There total 4 articles about (5RS,6RS)-1-Methyl-3-oxa-5-tosyloxy-6-<1'-<(methoxy)methoxy>cinnamyl>-6-methoxy-2-piperidinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 73062-21-2,73089-40-4,73089-41-5
(5RS,6RS)-1-Methyl-3-oxa-5-tosyloxy-6-(1'-hydroxycinnamyl)-6-methoxy-2-piperidinone

: 107-30-2
chloromethyl methyl ether

: 73089-58-4
(5RS,6RS)-1-Methyl-3-oxa-5-tosyloxy-6-<1'-<(methoxy)methoxy>cinnamyl>-6-methoxy-2-piperidinone

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 25 ℃; for 65h;
DOI:10.1021/jo01296a021

Reference yield:

: 73062-02-9
(5RS,6SR)-1-Methyl-3-oxa-5-hydroxy-6-cinnamoyl-6-methoxy-2-piperidinone

: 73089-58-4
(5RS,6RS)-1-Methyl-3-oxa-5-tosyloxy-6-<1'-<(methoxy)methoxy>cinnamyl>-6-methoxy-2-piperidinone

Guidance literature:: Multi-step reaction with 3 steps

1: pyridine / 25 °C

2: NaBH₄ / methanol / 0.18 h / 0 °C

3: 80 percent / Diisopropylethylamine / CH₂Cl₂ / 65 h / 25 °C

With sodium tetrahydroborate; N-ethyl-N,N-diisopropylamine; In pyridine; methanol; dichloromethane;
DOI:10.1021/jo01296a021

Reference yield:

: 73062-04-1
Toluene-4-sulfonic acid (4S,5R)-4-methoxy-3-methyl-2-oxo-4-[(E)-(3-phenyl-acryloyl)]-[1,3]oxazinan-5-yl ester

: 73089-58-4
(5RS,6RS)-1-Methyl-3-oxa-5-tosyloxy-6-<1'-<(methoxy)methoxy>cinnamyl>-6-methoxy-2-piperidinone

Guidance literature:: Multi-step reaction with 2 steps

1: NaBH₄ / methanol / 0.18 h / 0 °C

2: 80 percent / Diisopropylethylamine / CH₂Cl₂ / 65 h / 25 °C

With sodium tetrahydroborate; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane;
DOI:10.1021/jo01296a021