Decanethioic acid S-[(S)-1-hydroxymethyl-2-(4-phenoxy-benzyloxy)-ethyl] ester

Base Information

Chemical Name:Decanethioic acid S-[(S)-1-hydroxymethyl-2-(4-phenoxy-benzyloxy)-ethyl] ester
CAS No.:1025941-48-3
Molecular Formula:C₂₆H₃₆O₄S
Molecular Weight:444.635
Hs Code.:

Synonyms:Decanethioic acid S-[(S)-1-hydroxymethyl-2-(4-phenoxy-benzyloxy)-ethyl] ester

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Chemical Property of Decanethioic acid S-[(S)-1-hydroxymethyl-2-(4-phenoxy-benzyloxy)-ethyl] ester

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Technology Process of Decanethioic acid S-[(S)-1-hydroxymethyl-2-(4-phenoxy-benzyloxy)-ethyl] ester

There total 8 articles about Decanethioic acid S-[(S)-1-hydroxymethyl-2-(4-phenoxy-benzyloxy)-ethyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 161392-14-9
Decanethioic acid S-[(R)-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-1-(4-phenoxy-benzyloxymethyl)-ethyl] ester

: 1025941-48-3
Decanethioic acid S-[(S)-1-hydroxymethyl-2-(4-phenoxy-benzyloxy)-ethyl] ester

Guidance literature:: With toluene-4-sulfonic acid; In methanol; dichloromethane; at 25 ℃; for 1h;
DOI:10.1021/jm00050a009

Reference yield:

: 36881-42-2
1-(bromomethyl)-4-phenoxybenzene

: 1025941-48-3
Decanethioic acid S-[(S)-1-hydroxymethyl-2-(4-phenoxy-benzyloxy)-ethyl] ester

Guidance literature:: Multi-step reaction with 8 steps

1: 1.) NaH / 1.) DMF, 45 min, 2.) DMF, 25 deg C, 14 h

2: 1 N HCl / methanol / 24 h / 25 °C

3: pyridine / tetrahydrofuran / 14 h / 25 °C

4: pyridine / CH₂Cl₂ / 14 h / 25 °C

5: dimethylformamide / 16 h / 80 °C

6: NaBH₄ / ethanol / 1 h / 55 °C

7: pyridine / 14 h / 25 °C

8: p-toluenesulfonic acid / CH₂Cl₂; methanol / 1 h / 25 °C

With pyridine; hydrogenchloride; sodium tetrahydroborate; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00050a009

Reference yield:

: (R)-3-(4-Phenoxy-benzyloxy)-propane-1,2-diol

: 1025941-48-3
Decanethioic acid S-[(S)-1-hydroxymethyl-2-(4-phenoxy-benzyloxy)-ethyl] ester

Guidance literature:: Multi-step reaction with 6 steps

1: pyridine / tetrahydrofuran / 14 h / 25 °C

2: pyridine / CH₂Cl₂ / 14 h / 25 °C

3: dimethylformamide / 16 h / 80 °C

4: NaBH₄ / ethanol / 1 h / 55 °C

5: pyridine / 14 h / 25 °C

6: p-toluenesulfonic acid / CH₂Cl₂; methanol / 1 h / 25 °C

With pyridine; sodium tetrahydroborate; toluene-4-sulfonic acid; In tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00050a009