{ReCl(CNH-t-Bu)(CN-t-Bu)2(PMePh₂)2}SbF₆

Base Information

Chemical Name:{ReCl(CNH-t-Bu)(CN-t-Bu)2(PMePh₂)2}SbF₆
CAS No.:113380-16-8
Molecular Formula:C₄₁H₅₄ClN₃P₂Re*F₆Sb
Molecular Weight:1108.25
Hs Code.:

{ReCl(CNH-t-Bu)(CN-t-Bu)2(PMePh<sub>2</sub>)2}SbF<sub>6</sub>

Synonyms:{ReCl(CNH-t-Bu)(CN-t-Bu)2(PMePh₂)2}SbF₆

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Chemical Property of {ReCl(CNH-t-Bu)(CN-t-Bu)2(PMePh₂)2}SbF₆

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Technology Process of {ReCl(CNH-t-Bu)(CN-t-Bu)2(PMePh₂)2}SbF₆

There total 3 articles about {ReCl(CNH-t-Bu)(CN-t-Bu)2(PMePh₂)2}SbF₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 117408-26-1
{ReCl₂(CN-t-Bu)3(PMePh₂)2}SbF₆

: 113380-16-8
{ReCl(CNH-t-Bu)(CN-t-Bu)2(PMePh₂)2}SbF₆

Guidance literature:: With Al(s); In tetrahydrofuran; water; under N2, stirred and refluxed, 31 h;

Reference yield: 71.0%

: 113380-17-9
{ReCl₂(CN-t-Bu)3(PMePh₂)2}Cl

: 113380-16-8
{ReCl(CNH-t-Bu)(CN-t-Bu)2(PMePh₂)2}SbF₆

Guidance literature:: With Zn; KSbF₆; H₂O; zinc(II) chloride; In tetrahydrofuran; Excess Zn and KSbF6, traces H2O, refluxed, 6 h, N2-atmosphere.; Evapd., recrystd. from CH2Cl2/pentane, -30°C, elem., anal.;
DOI:10.1021/ja00216a062

Reference yield: 71.0%

: 16893-92-8
potassium hexafluoroantimonate

: 113380-17-9
{ReCl₂(CN-t-Bu)3(PMePh₂)2}Cl

: 113380-16-8
{ReCl(CNH-t-Bu)(CN-t-Bu)2(PMePh₂)2}SbF₆

Guidance literature:: With Zn(s); ZnCl₂; In tetrahydrofuran; water; under N2, stirred and refluxed, 6 h, mixture turned green, color change to yellow-green, monitored by thin-layer-chromy.; filtration, soln. concd. by bubbling N2, extn. (CH2Cl2, two times), soln. layered with pentane (-30°C, several d), filtrn., washed (pentane); elem. anal.;