ethyl N-<4-amino-1-(benzylideneamino)-2-(benzylthio)imidazo<4,5-c>pyridin-6-yl>carbamate

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Chemical Name:ethyl N-<4-amino-1-(benzylideneamino)-2-(benzylthio)imidazo<4,5-c>pyridin-6-yl>carbamate
CAS No.:123753-64-0
Molecular Formula:C₂₃H₂₂N₆O₂S
Molecular Weight:446.533
Hs Code.:

Synonyms:ethyl N-<4-amino-1-(benzylideneamino)-2-(benzylthio)imidazo<4,5-c>pyridin-6-yl>carbamate

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Chemical Property of ethyl N-<4-amino-1-(benzylideneamino)-2-(benzylthio)imidazo<4,5-c>pyridin-6-yl>carbamate

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Technology Process of ethyl N-<4-amino-1-(benzylideneamino)-2-(benzylthio)imidazo<4,5-c>pyridin-6-yl>carbamate

There total 4 articles about ethyl N-<4-amino-1-(benzylideneamino)-2-(benzylthio)imidazo<4,5-c>pyridin-6-yl>carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 123753-59-3
ethyl N-<4-amino-1-(benzylideneamino)-2(3H)-thioxo-imidazo<4,5-c>pyridin-6-yl>carbamate

: 100-44-7
benzyl chloride

: 123753-64-0
ethyl N-<4-amino-1-(benzylideneamino)-2-(benzylthio)imidazo<4,5-c>pyridin-6-yl>carbamate

Guidance literature:: With triethylamine; In N,N-dimethyl acetamide; for 20h; Ambient temperature;
DOI:10.1021/jm00164a030

Reference yield:

: 109182-40-3
ethyl (6-amino-4-hydrazino-5-nitropyridin-2-yl)carbamate

: 123753-64-0
ethyl N-<4-amino-1-(benzylideneamino)-2-(benzylthio)imidazo<4,5-c>pyridin-6-yl>carbamate

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / N,N-dimethyl-acetamide / 17 h / Ambient temperature

2: 83 percent / H₂ / Raney nickel / N,N-dimethyl-acetamide / 1.83 h / 760 Torr / Ambient temperature

3: 36 percent / Et₃N / N,N-dimethyl-acetamide / 23 h / Ambient temperature

4: 95 percent / Et₃N / N,N-dimethyl-acetamide / 20 h / Ambient temperature

With hydrogen; triethylamine; nickel; In N,N-dimethyl acetamide;
DOI:10.1021/jm00164a030

Reference yield:

: 123753-53-7
ethyl N-<6-amino-4-(2-benzylidenehydrazino)-5-nitropyridin-2-yl>carbamate

: 123753-64-0
ethyl N-<4-amino-1-(benzylideneamino)-2-(benzylthio)imidazo<4,5-c>pyridin-6-yl>carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 83 percent / H₂ / Raney nickel / N,N-dimethyl-acetamide / 1.83 h / 760 Torr / Ambient temperature

2: 36 percent / Et₃N / N,N-dimethyl-acetamide / 23 h / Ambient temperature

3: 95 percent / Et₃N / N,N-dimethyl-acetamide / 20 h / Ambient temperature

With hydrogen; triethylamine; nickel; In N,N-dimethyl acetamide;
DOI:10.1021/jm00164a030