hopyltriphenylphosphonium iodide

Base Information

• Chemical Name: hopyltriphenylphosphonium iodide
• CAS No.: 120446-13-1
• Molecular Formula: C₄₈H₆₆P*I
• Molecular Weight: 800.93
• Mol file: 120446-13-1.mol

Synonyms:hopyltriphenylphosphonium iodide

Chemical Property of hopyltriphenylphosphonium iodide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of hopyltriphenylphosphonium iodide

There total 3 articles about hopyltriphenylphosphonium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

hop-22(29)-ene (1615-91-4,1812-64-2,33323-60-3,33323-61-4,43206-60-6) → hopyltriphenylphosphonium iodide (120446-13-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 1.) borane-THF complex, 2.) 3 M aq. NaOH, 30percent H₂O₂ / 1.) THF, RT, 5 h, 2.) THF, 50 deg C, 3 h

2: 1.) triphenylphosphine (TPP), diethyl azodicarboxylate, 2.) MeI / 1.) THF, RT, 5 min, 2.) THF, 0.5 h

3: 12 h / 110 °C

With sodium hydroxide; borane-THF; dihydrogen peroxide; triphenylphosphine; diethylazodicarboxylate; methyl iodide;

Reference yield:

dryocrassol (34620-75-2,38706-33-1,59123-03-4,90319-98-5,107297-59-6) → hopyltriphenylphosphonium iodide (120446-13-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) triphenylphosphine (TPP), diethyl azodicarboxylate, 2.) MeI / 1.) THF, RT, 5 min, 2.) THF, 0.5 h

2: 12 h / 110 °C

With triphenylphosphine; diethylazodicarboxylate; methyl iodide;

Reference yield:

(3S,5aR,5bR,11aS,13bS)-3-(2-Iodo-1-methyl-ethyl)-5a,5b,8,8,11a,13b-hexamethyl-icosahydro-cyclopenta[a]chrysene + triphenylphosphine (603-35-0) → hopyltriphenylphosphonium iodide (120446-13-1)

Guidance literature:

at 110 ℃; for 12h;

upstream raw materials:

triphenylphosphine

hop-22⁽²⁹⁾-ene

dryocrassol