2-[(tert-butyl-diphenyl-silanyl)-methyl]-1-(toluene-4-sulfonyl)-azetidine

Base Information

• Chemical Name: 2-[(tert-butyl-diphenyl-silanyl)-methyl]-1-(toluene-4-sulfonyl)-azetidine
• CAS No.: 871906-59-1
• Molecular Formula: C₂₇H₃₃NO₂SSi
• Molecular Weight: 463.716

Synonyms:2-[(tert-butyl-diphenyl-silanyl)-methyl]-1-(toluene-4-sulfonyl)-azetidine

Chemical Property of 2-[(tert-butyl-diphenyl-silanyl)-methyl]-1-(toluene-4-sulfonyl)-azetidine

Chemical Property:

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Technology Process of 2-[(tert-butyl-diphenyl-silanyl)-methyl]-1-(toluene-4-sulfonyl)-azetidine

There total 1 articles about 2-[(tert-butyl-diphenyl-silanyl)-methyl]-1-(toluene-4-sulfonyl)-azetidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

2-[(tert-butyl-diphenyl-silanyl)-methyl]-1-(toluene-4-sulfonyl)-aziridine (871906-10-4) + trimethylsulfoxonium iodide (1774-47-6) → 2-[(tert-butyl-diphenyl-silanyl)-methyl]-1-(toluene-4-sulfonyl)-azetidine (871906-59-1)

Guidance literature:

trimethylsulfoxonium iodide; With sodium hydride; In tetrahydrofuran; N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

2-[(tert-butyl-diphenyl-silanyl)-methyl]-1-(toluene-4-sulfonyl)-aziridine; In tetrahydrofuran; N,N-dimethyl-formamide; at 110 ℃; for 7h;

DOI:10.1021/ja055664t

Reference yield: 92.0%

2-[(tert-butyl-diphenyl-silanyl)-methyl]-1-(toluene-4-sulfonyl)-azetidine (871906-59-1) → (+/-)-N-p-toluenesulfonyl-3-tert-butyldiphenylsilylmethyl pyrrolidine

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at 25 ℃; for 1h;

DOI:10.1021/ja055664t

Reference yield: 65.0%

2-[(tert-butyl-diphenyl-silanyl)-methyl]-1-(toluene-4-sulfonyl)-azetidine (871906-59-1) + acetonitrile (75-05-8,26809-02-9) → 4-[(tert-butyl-diphenyl-silanyl)-methyl]-2-methyl-1-(toluene-4-sulfonyl)-1,4,5,6-tetrahydro-pyrimidine

Guidance literature:

With boron trifluoride diethyl etherate; In dichloromethane; at 25 ℃; for 1h;

DOI:10.1021/ja055664t

upstream raw materials:

2-[(tert-butyl-diphenyl-silanyl)-methyl]-1-(toluene-4-sulfonyl)-aziridine

trimethylsulfoxonium iodide

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