N'-(4-dimethylaminobenzylidene)-9-methyl-1-(3-nitrophenyl)-β-carboline-3-carbohydrazide

Base Information

Chemical Name:N'-(4-dimethylaminobenzylidene)-9-methyl-1-(3-nitrophenyl)-β-carboline-3-carbohydrazide
CAS No.:1345667-87-9
Molecular Formula:C₂₈H₂₄N₆O₃
Molecular Weight:492.537
Hs Code.:

Synonyms:N'-(4-dimethylaminobenzylidene)-9-methyl-1-(3-nitrophenyl)-β-carboline-3-carbohydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N'-(4-dimethylaminobenzylidene)-9-methyl-1-(3-nitrophenyl)-β-carboline-3-carbohydrazide

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Technology Process of N'-(4-dimethylaminobenzylidene)-9-methyl-1-(3-nitrophenyl)-β-carboline-3-carbohydrazide

There total 6 articles about N'-(4-dimethylaminobenzylidene)-9-methyl-1-(3-nitrophenyl)-β-carboline-3-carbohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: C₁₉H₁₅N₅O₃

: 100-10-7
4-dimethylamino-benzaldehyde

: 1345667-87-9
N'-(4-dimethylaminobenzylidene)-9-methyl-1-(3-nitrophenyl)-β-carboline-3-carbohydrazide

Guidance literature:: With sulfuric acid; In ethanol; water; for 48h; Reflux;
DOI:10.1016/j.bmc.2011.08.059

Reference yield:

: 400782-57-2
methyl 1-(3-nitrophenyl)-9H-pyrido[3,4-b]indole-3-carboxylate

: 1345667-87-9
N'-(4-dimethylaminobenzylidene)-9-methyl-1-(3-nitrophenyl)-β-carboline-3-carbohydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / N,N-dimethyl-formamide / 48 h / 20 °C

2: hydrazine hydrate / ethanol / 72 h / Reflux

3: sulfuric acid / ethanol; water / 48 h / Reflux

With sulfuric acid; hydrazine hydrate; sodium hydroxide; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.08.059

Reference yield:

: 1-(3-nitrophenyl)-9H-β-carboline-3-carboxylic acid

: 1345667-87-9
N'-(4-dimethylaminobenzylidene)-9-methyl-1-(3-nitrophenyl)-β-carboline-3-carbohydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid

2: sodium hydroxide / N,N-dimethyl-formamide / 48 h / 20 °C

3: hydrazine hydrate / ethanol / 72 h / Reflux

4: sulfuric acid / ethanol; water / 48 h / Reflux

With sulfuric acid; hydrazine hydrate; sodium hydroxide; In ethanol; water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2011.08.059